6-[2-(2-methoxycarbonylphenylcarbamoyl)phenylcarbamoyl]-pyridine-2-carboxylic acid

Base Information

Chemical Name:6-[2-(2-methoxycarbonylphenylcarbamoyl)phenylcarbamoyl]-pyridine-2-carboxylic acid
CAS No.:196311-77-0
Molecular Formula:C₂₂H₁₇N₃O₆
Molecular Weight:419.393
Hs Code.:

Synonyms:6-[2-(2-methoxycarbonylphenylcarbamoyl)phenylcarbamoyl]-pyridine-2-carboxylic acid

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Chemical Property of 6-[2-(2-methoxycarbonylphenylcarbamoyl)phenylcarbamoyl]-pyridine-2-carboxylic acid

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Technology Process of 6-[2-(2-methoxycarbonylphenylcarbamoyl)phenylcarbamoyl]-pyridine-2-carboxylic acid

There total 4 articles about 6-[2-(2-methoxycarbonylphenylcarbamoyl)phenylcarbamoyl]-pyridine-2-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 196311-73-6
6-[2-(2-methoxycarbonylphenylcarbamoyl)phenylcarbamoyl]-pyridine-2-carboxylic acid benzyl ester

: 196311-77-0
6-[2-(2-methoxycarbonylphenylcarbamoyl)phenylcarbamoyl]-pyridine-2-carboxylic acid

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran; for 5h; Ambient temperature;
DOI:10.1021/ja963449u

Reference yield:

: 499-83-2
Pyridine-2,6-dicarboxylic acid

: 196311-77-0
6-[2-(2-methoxycarbonylphenylcarbamoyl)phenylcarbamoyl]-pyridine-2-carboxylic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 28 percent / Dowex 500-X₈ H⁺ / 1.5 h / Heating

2: TEA / pyridine / 3 h / Ambient temperature

3: 2.11 g / Et₃N / CH₂Cl₂ / Ambient temperature

4: 89 percent / H₂ / Pd/C / tetrahydrofuran / 5 h / Ambient temperature

With Dowex 500-X₈ H⁺; TEA; hydrogen; triethylamine; palladium on activated charcoal; In tetrahydrofuran; pyridine; dichloromethane;
DOI:10.1021/ja963449u

Reference yield:

: 125686-90-0
6-[(benzyloxy)carbonyl]pyridine-2-carboxylic acid

: 196311-77-0
6-[2-(2-methoxycarbonylphenylcarbamoyl)phenylcarbamoyl]-pyridine-2-carboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: TEA / pyridine / 3 h / Ambient temperature

2: 2.11 g / Et₃N / CH₂Cl₂ / Ambient temperature

3: 89 percent / H₂ / Pd/C / tetrahydrofuran / 5 h / Ambient temperature

With TEA; hydrogen; triethylamine; palladium on activated charcoal; In tetrahydrofuran; pyridine; dichloromethane;
DOI:10.1021/ja963449u