4-Methyl-benzenesulfinic acid [(R)-1-((S)-4-benzyl-5,6-dioxo-morpholin-3-yl)-2-methyl-propyl]-amide

Base Information

Chemical Name:4-Methyl-benzenesulfinic acid [(R)-1-((S)-4-benzyl-5,6-dioxo-morpholin-3-yl)-2-methyl-propyl]-amide
CAS No.:467471-41-6
Molecular Formula:C₂₂H₂₆N₂O₄S
Molecular Weight:414.525
Hs Code.:

Synonyms:4-Methyl-benzenesulfinic acid [(R)-1-((S)-4-benzyl-5,6-dioxo-morpholin-3-yl)-2-methyl-propyl]-amide

Suppliers and Price of 4-Methyl-benzenesulfinic acid [(R)-1-((S)-4-benzyl-5,6-dioxo-morpholin-3-yl)-2-methyl-propyl]-amide

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Chemical Property of 4-Methyl-benzenesulfinic acid [(R)-1-((S)-4-benzyl-5,6-dioxo-morpholin-3-yl)-2-methyl-propyl]-amide

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Technology Process of 4-Methyl-benzenesulfinic acid [(R)-1-((S)-4-benzyl-5,6-dioxo-morpholin-3-yl)-2-methyl-propyl]-amide

There total 1 articles about 4-Methyl-benzenesulfinic acid [(R)-1-((S)-4-benzyl-5,6-dioxo-morpholin-3-yl)-2-methyl-propyl]-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: 95-92-1
oxalic acid diethyl ester

: 467471-31-4
(+)-(2S,3R,S_S)-2-(benzylamino)-4-methyl-3-(p-tolylsulfinylamino)pentan-1-ol

: 467471-36-9
(+)-(5R,6S)-1-benzyl-6-hydroxymethyl-5-(i-propyl)piperazine-2,3-dione

: 467471-41-6
4-Methyl-benzenesulfinic acid [(R)-1-((S)-4-benzyl-5,6-dioxo-morpholin-3-yl)-2-methyl-propyl]-amide

Guidance literature:: With sodium methylate; In methanol; dichloromethane; at 20 ℃;
DOI:10.1055/s-2002-25336

Reference yield:

: 467471-41-6
4-Methyl-benzenesulfinic acid [(R)-1-((S)-4-benzyl-5,6-dioxo-morpholin-3-yl)-2-methyl-propyl]-amide

: 467471-36-9
(+)-(5R,6S)-1-benzyl-6-hydroxymethyl-5-(i-propyl)piperazine-2,3-dione

Guidance literature:: With sodium methylate; In methanol; for 1h;
DOI:10.1055/s-2002-25336

Reference yield:

: 467471-41-6
4-Methyl-benzenesulfinic acid [(R)-1-((S)-4-benzyl-5,6-dioxo-morpholin-3-yl)-2-methyl-propyl]-amide

: (-)-(2S,3R)-1-benzyl-2-hydroxymethyl-3-i-propylpiperazine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium methoxide / methanol / 72 h / 20 °C

2: 61 percent / borane dimethyl sulfide complex / tetrahydrofuran / 7 h / Heating

With dimethylsulfide borane complex; sodium methylate; In tetrahydrofuran; methanol;
DOI:10.1021/jo052077h