methyl 6-({[(1,1-dimethylethyl)oxy]carbonyl}amino)-2,3-difluorobenzoate

Base Information

Chemical Name:methyl 6-({[(1,1-dimethylethyl)oxy]carbonyl}amino)-2,3-difluorobenzoate
CAS No.:1116228-29-5
Molecular Formula:C₁₃H₁₅F₂NO₄
Molecular Weight:287.263
Hs Code.:

Synonyms:methyl 6-({[(1,1-dimethylethyl)oxy]carbonyl}amino)-2,3-difluorobenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 6-({[(1,1-dimethylethyl)oxy]carbonyl}amino)-2,3-difluorobenzoate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of methyl 6-({[(1,1-dimethylethyl)oxy]carbonyl}amino)-2,3-difluorobenzoate

There total 1 articles about methyl 6-({[(1,1-dimethylethyl)oxy]carbonyl}amino)-2,3-difluorobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 144298-04-4
(3,4-difluorophenyl)-carbamic acid-tert-butyl ester

: 79-22-1
methyl chloroformate

: 1116228-29-5
methyl 6-({[(1,1-dimethylethyl)oxy]carbonyl}amino)-2,3-difluorobenzoate

Guidance literature:: (3,4-difluorophenyl)-carbamic acid-tert-butyl ester; With tert.-butyl lithium; In tetrahydrofuran; pentane; at -78 ℃; for 3h;

methyl chloroformate; In tetrahydrofuran; pentane; at -78 ℃; for 0.75h;

With water; ammonium chloride; In tetrahydrofuran; pentane; at -78 ℃;

Reference yield:

: 1116228-29-5
methyl 6-({[(1,1-dimethylethyl)oxy]carbonyl}amino)-2,3-difluorobenzoate

: 442134-72-7
2,3-difluoro-6-aminobenzoic acid

Guidance literature:: methyl 6-({[(1,1-dimethylethyl)oxy]carbonyl}amino)-2,3-difluorobenzoate; With trifluoroacetic acid; In dichloromethane; at 20 ℃;

With lithium hydroxide; water; In tetrahydrofuran; at 20 ℃;

With hydrogenchloride; In tetrahydrofuran; water; ethyl acetate; at 20 ℃; pH=7;