methyl 6-heptyl-5-iodo-4-(2-iodo-5-methoxy-3-methyl-4-nitrophenoxy)-2-methoxybenzoate

Base Information

Chemical Name:methyl 6-heptyl-5-iodo-4-(2-iodo-5-methoxy-3-methyl-4-nitrophenoxy)-2-methoxybenzoate
CAS No.:93796-80-6
Molecular Formula:C₂₄H₂₉I₂NO₇
Molecular Weight:697.306
Hs Code.:

Synonyms:methyl 6-heptyl-5-iodo-4-(2-iodo-5-methoxy-3-methyl-4-nitrophenoxy)-2-methoxybenzoate

Suppliers and Price of methyl 6-heptyl-5-iodo-4-(2-iodo-5-methoxy-3-methyl-4-nitrophenoxy)-2-methoxybenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 6-heptyl-5-iodo-4-(2-iodo-5-methoxy-3-methyl-4-nitrophenoxy)-2-methoxybenzoate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of methyl 6-heptyl-5-iodo-4-(2-iodo-5-methoxy-3-methyl-4-nitrophenoxy)-2-methoxybenzoate

There total 8 articles about methyl 6-heptyl-5-iodo-4-(2-iodo-5-methoxy-3-methyl-4-nitrophenoxy)-2-methoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 93796-79-3
methyl 6-heptyl-5-iodo-2-methoxy-4-(3-methoxy-5-methyl-4-nitrophenoxy)benzoate

: 93796-80-6
methyl 6-heptyl-5-iodo-4-(2-iodo-5-methoxy-3-methyl-4-nitrophenoxy)-2-methoxybenzoate

Guidance literature:: With iodine; silver trifluoroacetate; In chloroform; for 20h;

Reference yield:

: 74204-00-5
3-bromo-5-methylphenol

: 93796-80-6
methyl 6-heptyl-5-iodo-4-(2-iodo-5-methoxy-3-methyl-4-nitrophenoxy)-2-methoxybenzoate

Guidance literature:: Multi-step reaction with 5 steps

1: 22 percent / nitric acid, acetic acid / 4 h / 15 - 16 °C / further nitration agents

2: potassium carbonate / dimethylformamide / Ambient temperature

3: 61 percent / potassium carbonate, copper(II) oxide / 16 h / 140 °C

4: 92 percent / iodine, silver trifluoroacetate / CHCl₃

5: 97 percent / iodine, silver trifluoroacetate / CHCl₃ / 20 h

With iodine; nitric acid; silver trifluoroacetate; potassium carbonate; acetic acid; copper(II) oxide; In chloroform; N,N-dimethyl-formamide;

Reference yield:

: 108-39-4
3-methyl-phenol

: 93796-80-6
methyl 6-heptyl-5-iodo-4-(2-iodo-5-methoxy-3-methyl-4-nitrophenoxy)-2-methoxybenzoate

Guidance literature:: Multi-step reaction with 7 steps

1: 77 percent / bromine, aluminium powder

2: 83 percent / aluminium chloride / benzene / 0.5 h / Heating

3: 22 percent / nitric acid, acetic acid / 4 h / 15 - 16 °C / further nitration agents

4: potassium carbonate / dimethylformamide / Ambient temperature

5: 61 percent / potassium carbonate, copper(II) oxide / 16 h / 140 °C

6: 92 percent / iodine, silver trifluoroacetate / CHCl₃

7: 97 percent / iodine, silver trifluoroacetate / CHCl₃ / 20 h

With aluminium trichloride; bromine; iodine; nitric acid; silver trifluoroacetate; potassium carbonate; acetic acid; aluminium; copper(II) oxide; In chloroform; N,N-dimethyl-formamide; benzene;