C₃₄H₄₆O₄Si

Base Information

• Chemical Name: C₃₄H₄₆O₄Si
• CAS No.: 1374425-47-4
• Molecular Formula: C₃₄H₄₆O₄Si
• Molecular Weight: 546.822

Synonyms:C₃₄H₄₆O₄Si

Chemical Property of C₃₄H₄₆O₄Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Technology Process of C₃₄H₄₆O₄Si

There total 20 articles about C₃₄H₄₆O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C13H20O5 → C34H46O4Si (1374425-47-4)

Guidance literature:

Multi-step reaction with 15 steps

1.1: methanol; diethyl ether; toluene / 0.25 h / Inert atmosphere

2.1: lithium aluminium tetrahydride / tetrahydrofuran; dichloromethane / 0.5 h / 0 °C / Inert atmosphere

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C / Inert atmosphere

3.2: 16 h / 20 °C / Inert atmosphere

4.1: toluene-4-sulfonic acid / water; acetone / 0.5 h / 20 °C

5.1: triethylamine / dichloromethane / 0.75 h / 0 °C / Inert atmosphere

6.1: oxygen; palladium diacetate / dimethyl sulfoxide / 16 h / 20 - 80 °C

7.1: iodine; magnesium / tetrahydrofuran / 2 h / 70 °C / Inert atmosphere

7.2: 0.5 h / -78 °C / Inert atmosphere

7.3: 5 h / -78 °C / Inert atmosphere

8.1: toluene-4-sulfonic acid / acetone / 0.5 h / 20 °C / Inert atmosphere

9.1: n-butyllithium; lithium diisopropyl amide / tetrahydrofuran; cyclohexane / 1 h / -78 °C / Inert atmosphere

9.2: 3 h / -78 °C / Inert atmosphere

10.1: pyridine; dihydrogen peroxide / dichloromethane; water / 0.5 h / 0 - 20 °C

11.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.25 h / -78 °C / Inert atmosphere

12.1: 1,2-dichloro-benzene / 1 h / 220 °C / Microwave irradiation; Inert atmosphere

13.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

13.2: 0.5 h / -78 - 20 °C / Inert atmosphere

14.1: water; iodine / tetrahydrofuran / 16 h / 20 °C

15.1: triethyl borane; tri-n-butyl-tin hydride / hexane; toluene / 1 h / -78 °C / Air

With pyridine; lithium aluminium tetrahydride; n-butyllithium; triethyl borane; water; dihydrogen peroxide; iodine; oxygen; tri-n-butyl-tin hydride; palladium diacetate; sodium hydride; diisobutylaluminium hydride; toluene-4-sulfonic acid; magnesium; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; cyclohexane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; 1,2-dichloro-benzene; acetone; toluene; mineral oil;

DOI:10.1002/ejoc.201101629

Reference yield:

C13H20O3 (1374425-20-3) → C34H46O4Si (1374425-47-4)

Guidance literature:

Multi-step reaction with 17 steps

1.1: triethylamine / dichloromethane / 3 h / -78 °C / Inert atmosphere

2.1: ozone / dichloromethane / 3 h / -78 °C

2.2: 4 h / 20 °C / Inert atmosphere

3.1: methanol; diethyl ether; toluene / 0.25 h / Inert atmosphere

4.1: lithium aluminium tetrahydride / tetrahydrofuran; dichloromethane / 0.5 h / 0 °C / Inert atmosphere

5.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C / Inert atmosphere

5.2: 16 h / 20 °C / Inert atmosphere

6.1: toluene-4-sulfonic acid / water; acetone / 0.5 h / 20 °C

7.1: triethylamine / dichloromethane / 0.75 h / 0 °C / Inert atmosphere

8.1: oxygen; palladium diacetate / dimethyl sulfoxide / 16 h / 20 - 80 °C

9.1: iodine; magnesium / tetrahydrofuran / 2 h / 70 °C / Inert atmosphere

9.2: 0.5 h / -78 °C / Inert atmosphere

9.3: 5 h / -78 °C / Inert atmosphere

10.1: toluene-4-sulfonic acid / acetone / 0.5 h / 20 °C / Inert atmosphere

11.1: n-butyllithium; lithium diisopropyl amide / tetrahydrofuran; cyclohexane / 1 h / -78 °C / Inert atmosphere

11.2: 3 h / -78 °C / Inert atmosphere

12.1: pyridine; dihydrogen peroxide / dichloromethane; water / 0.5 h / 0 - 20 °C

13.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.25 h / -78 °C / Inert atmosphere

14.1: 1,2-dichloro-benzene / 1 h / 220 °C / Microwave irradiation; Inert atmosphere

15.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

15.2: 0.5 h / -78 - 20 °C / Inert atmosphere

16.1: water; iodine / tetrahydrofuran / 16 h / 20 °C

17.1: triethyl borane; tri-n-butyl-tin hydride / hexane; toluene / 1 h / -78 °C / Air

With pyridine; lithium aluminium tetrahydride; n-butyllithium; triethyl borane; water; dihydrogen peroxide; iodine; oxygen; tri-n-butyl-tin hydride; palladium diacetate; sodium hydride; diisobutylaluminium hydride; toluene-4-sulfonic acid; ozone; magnesium; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; cyclohexane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; 1,2-dichloro-benzene; acetone; toluene; mineral oil;

DOI:10.1002/ejoc.201101629

Reference yield:

C16H28O3Si → C34H46O4Si (1374425-47-4)

Guidance literature:

Multi-step reaction with 16 steps

1.1: ozone / dichloromethane / 3 h / -78 °C

1.2: 4 h / 20 °C / Inert atmosphere

2.1: methanol; diethyl ether; toluene / 0.25 h / Inert atmosphere

3.1: lithium aluminium tetrahydride / tetrahydrofuran; dichloromethane / 0.5 h / 0 °C / Inert atmosphere

4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C / Inert atmosphere

4.2: 16 h / 20 °C / Inert atmosphere

5.1: toluene-4-sulfonic acid / water; acetone / 0.5 h / 20 °C

6.1: triethylamine / dichloromethane / 0.75 h / 0 °C / Inert atmosphere

7.1: oxygen; palladium diacetate / dimethyl sulfoxide / 16 h / 20 - 80 °C

8.1: iodine; magnesium / tetrahydrofuran / 2 h / 70 °C / Inert atmosphere

8.2: 0.5 h / -78 °C / Inert atmosphere

8.3: 5 h / -78 °C / Inert atmosphere

9.1: toluene-4-sulfonic acid / acetone / 0.5 h / 20 °C / Inert atmosphere

10.1: n-butyllithium; lithium diisopropyl amide / tetrahydrofuran; cyclohexane / 1 h / -78 °C / Inert atmosphere

10.2: 3 h / -78 °C / Inert atmosphere

11.1: pyridine; dihydrogen peroxide / dichloromethane; water / 0.5 h / 0 - 20 °C

12.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.25 h / -78 °C / Inert atmosphere

13.1: 1,2-dichloro-benzene / 1 h / 220 °C / Microwave irradiation; Inert atmosphere

14.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

14.2: 0.5 h / -78 - 20 °C / Inert atmosphere

15.1: water; iodine / tetrahydrofuran / 16 h / 20 °C

16.1: triethyl borane; tri-n-butyl-tin hydride / hexane; toluene / 1 h / -78 °C / Air

With pyridine; lithium aluminium tetrahydride; n-butyllithium; triethyl borane; water; dihydrogen peroxide; iodine; oxygen; tri-n-butyl-tin hydride; palladium diacetate; sodium hydride; diisobutylaluminium hydride; toluene-4-sulfonic acid; ozone; magnesium; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; cyclohexane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; 1,2-dichloro-benzene; acetone; toluene; mineral oil;

DOI:10.1002/ejoc.201101629

upstream raw materials:

C₂₅H₃₀O₃

C₃₅H₅₂O₃Si₂

C₃₂H₄₄O₃Si

C₃₂H₄₂O₃Si

Downstream raw materials:

C₃₄H₅₀O₄Si

C₃₈H₄₆O₄

C₃₇H₄₆O₅

C₃₇H₄₄O₅

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