4-acetyl-2,6-dibenzoyl-4-ethoxycarbonyl-3,5-diphenylthiane

Base Information

• Chemical Name: 4-acetyl-2,6-dibenzoyl-4-ethoxycarbonyl-3,5-diphenylthiane
• CAS No.: 1184937-93-6
• Molecular Formula: C₃₆H₃₂O₅S
• Molecular Weight: 576.713
• Mol file: 1184937-93-6.mol

Synonyms:4-acetyl-2,6-dibenzoyl-4-ethoxycarbonyl-3,5-diphenylthiane

Chemical Property of 4-acetyl-2,6-dibenzoyl-4-ethoxycarbonyl-3,5-diphenylthiane

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 4-acetyl-2,6-dibenzoyl-4-ethoxycarbonyl-3,5-diphenylthiane

There total 2 articles about 4-acetyl-2,6-dibenzoyl-4-ethoxycarbonyl-3,5-diphenylthiane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

(Z,Z)-2,2'-thiobis(1,3-diphenylprop-2-en-1-one) (148638-23-7) + ethyl acetoacetate (141-97-9) → trans-5-benzoyl-2-methyl-4-phenyl-4,5-dihydrofuran-3-carboxylic acid ethyl ester + 4-acetyl-2,6-dibenzoyl-4-ethoxycarbonyl-3,5-diphenylthiane (1184937-93-6)

Guidance literature:

ethyl acetoacetate; With ethanol; sodium ethanolate;

(Z,Z)-2,2'-thiobis(1,3-diphenylprop-2-en-1-one); In ethanol; N,N-dimethyl-formamide; at 20 ℃; for 1h; stereoselective reaction;

DOI:10.1080/00397910802664236

Reference yield: 15.0%

(Z,Z)-2,2'-thiobis(1,3-diphenylprop-2-en-1-one) (148638-23-7) + ethyl acetoacetate (141-97-9) → trans-5-benzoyl-2-methyl-4-phenyl-4,5-dihydrofuran-3-carboxylic acid ethyl ester + 4-acetyl-2,6-dibenzoyl-4-ethoxycarbonyl-3,5-diphenylthiane (1184937-93-6) + benzalacetophenone (94-41-7)

Guidance literature:

ethyl acetoacetate; With ethanol; sodium ethanolate;

(Z,Z)-2,2'-thiobis(1,3-diphenylprop-2-en-1-one); In ethanol; N,N-dimethyl-formamide; at 20 ℃; for 1h; stereoselective reaction;

DOI:10.1080/00397910802664236

upstream raw materials:

(Z,Z)-2,2'-thiobis(1,3-diphenylprop-2-en-1-one)

ethyl acetoacetate