exo methyl rocaglate

Base Information

• Chemical Name: exo methyl rocaglate
• CAS No.: 901774-43-4
• Molecular Formula: C₂₈H₂₈O₈
• Molecular Weight: 492.526

Synonyms:exo methyl rocaglate

Chemical Property of exo methyl rocaglate

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of exo methyl rocaglate

There total 3 articles about exo methyl rocaglate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

keto rocaglate (901774-46-7) → exo methyl rocaglate (901774-43-4) + aglafoline (143901-35-3)

Guidance literature:

keto rocaglate; With acetic acid; tetramethylammonium triacetoxyborohydride; In acetonitrile; at 20 ℃; for 3h;

With ammonium chloride; In water; acetonitrile;

With sodium L-tartrate; potassium L-tartrate; In water; acetonitrile; at 20 ℃; for 0.5h;

Reference yield:

keto rocaglate (901774-46-7) → exo methyl rocaglate (901774-43-4) + (ent)-exo methyl rocaglate + (ent)-endo methyl rocaglate + aglafoline (143901-35-3)

Guidance literature:

With acetic acid; tetramethylammonium triacetoxyborohydride; In acetonitrile; at 20 ℃; for 3h;

DOI:10.1021/ja062621j

Reference yield:

trimethoxy cyclopenta[bc]benzopyran → exo methyl rocaglate (901774-43-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 95 percent / NaOMe / methanol / 0.33 h / 60 °C

2: Me₄NBH(OAc)3; acetic acid / acetonitrile / 3 h / 20 °C

With sodium methylate; acetic acid; tetramethylammonium triacetoxyborohydride; In methanol; acetonitrile;

DOI:10.1021/ja062621j

upstream raw materials:

keto rocaglate

Downstream raw materials:

exo rocaglic acid

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