(E)-N-[3-[4-(1'-deoxy-2',3',4',6'-tetra-O-acetyl-β-D-glucopyranos-1'-yl)-3-oxobut-1-enyl]phenyl]-2-carbamoylbenzoic acid

Base Information

Chemical Name:(E)-N-[3-[4-(1'-deoxy-2',3',4',6'-tetra-O-acetyl-β-D-glucopyranos-1'-yl)-3-oxobut-1-enyl]phenyl]-2-carbamoylbenzoic acid
CAS No.:1426398-82-4
Molecular Formula:C₃₂H₃₃NO₁₃
Molecular Weight:639.613
Hs Code.:

Synonyms:(E)-N-[3-[4-(1'-deoxy-2',3',4',6'-tetra-O-acetyl-β-D-glucopyranos-1'-yl)-3-oxobut-1-enyl]phenyl]-2-carbamoylbenzoic acid

Suppliers and Price of (E)-N-[3-[4-(1'-deoxy-2',3',4',6'-tetra-O-acetyl-β-D-glucopyranos-1'-yl)-3-oxobut-1-enyl]phenyl]-2-carbamoylbenzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (E)-N-[3-[4-(1'-deoxy-2',3',4',6'-tetra-O-acetyl-β-D-glucopyranos-1'-yl)-3-oxobut-1-enyl]phenyl]-2-carbamoylbenzoic acid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (E)-N-[3-[4-(1'-deoxy-2',3',4',6'-tetra-O-acetyl-β-D-glucopyranos-1'-yl)-3-oxobut-1-enyl]phenyl]-2-carbamoylbenzoic acid

There total 2 articles about (E)-N-[3-[4-(1'-deoxy-2',3',4',6'-tetra-O-acetyl-β-D-glucopyranos-1'-yl)-3-oxobut-1-enyl]phenyl]-2-carbamoylbenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 85-44-9
phthalic anhydride

: 1426398-75-5
(E)-4-(3-aminophenyl)-1-[1'-deoxy-2',3',4',6'-tetra-O-acetyl-β-D-glucopyranos-1'-yl]but-3-en-2-one

: 1426398-82-4
(E)-N-[3-[4-(1'-deoxy-2',3',4',6'-tetra-O-acetyl-β-D-glucopyranos-1'-yl)-3-oxobut-1-enyl]phenyl]-2-carbamoylbenzoic acid

Guidance literature:: In acetone; at 20 ℃;
DOI:10.3998/ark.5550190.0014.213

Reference yield:

: 99-61-6
3-nitro-benzaldehyde

: 1426398-82-4
(E)-N-[3-[4-(1'-deoxy-2',3',4',6'-tetra-O-acetyl-β-D-glucopyranos-1'-yl)-3-oxobut-1-enyl]phenyl]-2-carbamoylbenzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: pyrrolidine / dichloromethane / 20 °C

2: tin(II) chloride dihdyrate / ethanol / 120 h / 30 °C / Sonication

3: acetone / 20 °C

With pyrrolidine; tin(II) chloride dihdyrate; In ethanol; dichloromethane; acetone;
DOI:10.3998/ark.5550190.0014.213