Technology Process of C31H35N3O6S2
There total 7 articles about C31H35N3O6S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C33H39N3O6S2;
With
potassium hydroxide;
In
ethanol; ethyl acetate;
for 2h;
With
hydrogenchloride;
In
ethanol; water; ethyl acetate;
pH=3 - 4;
DOI:10.1002/chem.201103191
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: tin(ll) chloride / ethanol; acetonitrile / 12 h / Reflux
2.1: benzotriazol-1-ol; dicyclohexyl-carbodiimide / dichloromethane / 0.5 h / 20 °C
2.2: Inert atmosphere
3.1: potassium hydroxide / ethanol; ethyl acetate / 2 h
3.2: pH 3 - 4
With
benzotriazol-1-ol; dicyclohexyl-carbodiimide; tin(ll) chloride; potassium hydroxide;
In
ethanol; dichloromethane; ethyl acetate; acetonitrile;
DOI:10.1002/chem.201103191
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: benzotriazol-1-ol; dicyclohexyl-carbodiimide / dichloromethane / 0.5 h / 20 °C
1.2: Inert atmosphere
2.1: potassium hydroxide / ethanol; ethyl acetate / 2 h
2.2: pH 3 - 4
With
benzotriazol-1-ol; dicyclohexyl-carbodiimide; potassium hydroxide;
In
ethanol; dichloromethane; ethyl acetate;
DOI:10.1002/chem.201103191