3-Butenoic acid, 3-Methyl-, phenylMethyl ester

Base Information

Chemical Name:3-Butenoic acid, 3-Methyl-, phenylMethyl ester
CAS No.:37526-86-6
Molecular Formula:C₁₂H₁₄O₂
Molecular Weight:190.242
Hs Code.:
Mol file:37526-86-6.mol

Synonyms:benzyl 3-methylbut-3-enoate

Suppliers and Price of 3-Butenoic acid, 3-Methyl-, phenylMethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of 3-Butenoic acid, 3-Methyl-, phenylMethyl ester

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

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Hazard Codes:

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Technology Process of 3-Butenoic acid, 3-Methyl-, phenylMethyl ester

There total 6 articles about 3-Butenoic acid, 3-Methyl-, phenylMethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 140-18-1
Benzyl chloroacetate

: potassium isopropenyltrifluoroborane

: 37526-86-6
benzyl 3-methylbut-3-enoate

Guidance literature:: With chloro(2-dicyclohexylphosphino-2’,4’,6’-triisopropyl-1,1‘-biphenyl)[2-(2’-amino-1,1‘-biphenyl’)]palladium(II); potassium carbonate; In tetrahydrofuran; water; at 80 ℃; for 12h; stereoselective reaction; Inert atmosphere;
DOI:10.1021/ol401377q

Reference yield:

: 1617-31-8
3-methylbut-3-enoic acid

: 100-51-6,185532-71-2
benzyl alcohol

: 37526-86-6
benzyl 3-methylbut-3-enoate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; Schlenk technique; Cooling with ice;
DOI:10.1039/c4cc00148f