(2R,3R)-3-hydroxy-2-methyltridecanoic acid (1R,2S)-2-[benzyl-(2,4,6-trimethyl-benzenesulfonyl)amino]-1-phenylpropyl ester

Base Information

Chemical Name:(2R,3R)-3-hydroxy-2-methyltridecanoic acid (1R,2S)-2-[benzyl-(2,4,6-trimethyl-benzenesulfonyl)amino]-1-phenylpropyl ester
CAS No.:694527-59-8
Molecular Formula:C₃₉H₅₅NO₅S
Molecular Weight:649.935
Hs Code.:

Synonyms:(2R,3R)-3-hydroxy-2-methyltridecanoic acid (1R,2S)-2-[benzyl-(2,4,6-trimethyl-benzenesulfonyl)amino]-1-phenylpropyl ester

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Chemical Property of (2R,3R)-3-hydroxy-2-methyltridecanoic acid (1R,2S)-2-[benzyl-(2,4,6-trimethyl-benzenesulfonyl)amino]-1-phenylpropyl ester

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Technology Process of (2R,3R)-3-hydroxy-2-methyltridecanoic acid (1R,2S)-2-[benzyl-(2,4,6-trimethyl-benzenesulfonyl)amino]-1-phenylpropyl ester

There total 1 articles about (2R,3R)-3-hydroxy-2-methyltridecanoic acid (1R,2S)-2-[benzyl-(2,4,6-trimethyl-benzenesulfonyl)amino]-1-phenylpropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 112-44-7
undecylaldehyde

: 187324-66-9
(1R,2S)-2-(N-benzyl-N-mesitylenesulfonyl)amino-1-phenyl-1-propyl propionate

: 3-hydroxy-2-methyltridecanoic acid (1R,2S)-2-[benzyl-(2,4,6-trimethyl-benzenesulfonyl)amino]-1-phenylpropyl ester

: 694527-59-8
(2R,3R)-3-hydroxy-2-methyltridecanoic acid (1R,2S)-2-[benzyl-(2,4,6-trimethyl-benzenesulfonyl)amino]-1-phenylpropyl ester

Guidance literature:: (1R,2S)-2-(N-benzyl-N-mesitylenesulfonyl)amino-1-phenyl-1-propyl propionate; With triethylamine; dicyclohexyl(((trifluoromethyl)sulfonyl)oxy)borane; In hexane; dichloromethane; at -78 ℃; for 2h;

undecylaldehyde; In hexane; dichloromethane; at -78 - 0 ℃; for 6h;
DOI:10.1016/j.bmc.2003.10.055

Reference yield:

: 694527-59-8
(2R,3R)-3-hydroxy-2-methyltridecanoic acid (1R,2S)-2-[benzyl-(2,4,6-trimethyl-benzenesulfonyl)amino]-1-phenylpropyl ester

: 694527-81-6
N-((2R,3R)-3-hydroxy-2-methyltridecanoyl)-N-Me-L-Leu-L-allo-Ile-L-Ser(Bn)-OAllyl

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / LiOH*H₂O / tetrahydrofuran; methanol; H₂O / 20 °C

2: 99 percent / Et₃N; diethylcyanophosphate / tetrahydrofuran / 16 h / 0 - 20 °C

With lithium hydroxide; diethyl cyanophosphonate; triethylamine; In tetrahydrofuran; methanol; water;
DOI:10.1016/j.bmc.2003.10.055