5-Isopropyl-6-methanesulfonyl-1-(2-m-tolyl-ethoxy)-1H-pyrimidine-2,4-dione

Base Information

Chemical Name:5-Isopropyl-6-methanesulfonyl-1-(2-m-tolyl-ethoxy)-1H-pyrimidine-2,4-dione
CAS No.:191472-67-0
Molecular Formula:C₁₇H₂₂N₂O₅S
Molecular Weight:366.438
Hs Code.:

Synonyms:5-Isopropyl-6-methanesulfonyl-1-(2-m-tolyl-ethoxy)-1H-pyrimidine-2,4-dione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-Isopropyl-6-methanesulfonyl-1-(2-m-tolyl-ethoxy)-1H-pyrimidine-2,4-dione

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Technology Process of 5-Isopropyl-6-methanesulfonyl-1-(2-m-tolyl-ethoxy)-1H-pyrimidine-2,4-dione

There total 9 articles about 5-Isopropyl-6-methanesulfonyl-1-(2-m-tolyl-ethoxy)-1H-pyrimidine-2,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 191472-41-0
5-Isopropyl-6-methylsulfanyl-1-(2-m-tolyl-ethoxy)-1H-pyrimidine-2,4-dione

: 191472-67-0
5-Isopropyl-6-methanesulfonyl-1-(2-m-tolyl-ethoxy)-1H-pyrimidine-2,4-dione

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 16h; Heating;
DOI:10.1021/jm9607921

Reference yield:

: 1875-89-4
2-(3-methylphenyl)ethanol

: 191472-67-0
5-Isopropyl-6-methanesulfonyl-1-(2-m-tolyl-ethoxy)-1H-pyrimidine-2,4-dione

Guidance literature:: Multi-step reaction with 5 steps

1: 96 percent / diethyl azodicarboxylate, triphenylphosphine / tetrahydrofuran / 16 h / Ambient temperature

2: 89 percent / hydrazine monohydrate / methanol / 4 h / Heating

3: benzene / 1 h / Ambient temperature

4: 96 percent / p-TsOH, AcOH / 1 h / 80 °C

5: 86 percent / 3-chloroperoxybenzoic acid / CH₂Cl₂ / 16 h / Heating

With toluene-4-sulfonic acid; hydrazine hydrate; acetic acid; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol; dichloromethane; benzene;
DOI:10.1021/jm9607921

Reference yield:

: 132767-06-7
ethyl 3,3-bis(methylthio)-2-isopropylacrylate

: 191472-67-0
5-Isopropyl-6-methanesulfonyl-1-(2-m-tolyl-ethoxy)-1H-pyrimidine-2,4-dione

Guidance literature:: Multi-step reaction with 6 steps

1: 82 percent / 2 N KOH in EtOH / 3 h / Heating

2: 91 percent / oxalyl chloride, DMF / benzene / 3 h / Ambient temperature

3: benzene / 0.5 h / Heating

4: benzene / 1 h / Ambient temperature

5: 96 percent / p-TsOH, AcOH / 1 h / 80 °C

6: 86 percent / 3-chloroperoxybenzoic acid / CH₂Cl₂ / 16 h / Heating

With potassium hydroxide; oxalyl dichloride; toluene-4-sulfonic acid; acetic acid; N,N-dimethyl-formamide; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; benzene;
DOI:10.1021/jm9607921