2,8-diketo-9-(4-methoxybenzyl)-10-(1-methylethenyl)-1-benzyl-3,9-diazatricyclo<5.2.2.0^3,7>undecane

Base Information

• Chemical Name: 2,8-diketo-9-(4-methoxybenzyl)-10-(1-methylethenyl)-1-benzyl-3,9-diazatricyclo<5.2.2.0^3,7>undecane
• CAS No.: 124375-85-5
• Molecular Formula: C₂₇H₃₀N₂O₃
• Molecular Weight: 430.547

Synonyms:2,8-diketo-9-(4-methoxybenzyl)-10-(1-methylethenyl)-1-benzyl-3,9-diazatricyclo<5.2.2.0^3,7>undecane

Chemical Property of 2,8-diketo-9-(4-methoxybenzyl)-10-(1-methylethenyl)-1-benzyl-3,9-diazatricyclo<5.2.2.0^3,7>undecane

Chemical Property:

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Technology Process of 2,8-diketo-9-(4-methoxybenzyl)-10-(1-methylethenyl)-1-benzyl-3,9-diazatricyclo<5.2.2.0^3,7>undecane

There total 11 articles about 2,8-diketo-9-(4-methoxybenzyl)-10-(1-methylethenyl)-1-benzyl-3,9-diazatricyclo<5.2.2.0^3,7>undecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

6-<(2E)-4-chloro-3-methylbut-2-enyl>-2,5-diketo-4-(4-methoxybenzyl)-3-benzyl-1,4-diazabicyclo<4.3.0>nonane (124268-80-0) → 2,8-diketo-9-(4-methoxybenzyl)-10-(1-methylethenyl)-1-benzyl-3,9-diazatricyclo<5.2.2.03,7>undecane (124375-85-5) + (1R,7R,11R)-7-Benzyl-11-isopropenyl-8-(4-methoxy-benzyl)-5,8-diaza-tricyclo[5.2.2.01,5]undecane-6,9-dione (124268-81-1,124375-85-5)

Guidance literature:

With sodium hydride; In hexane; N,N-dimethyl-formamide; Ambient temperature;

Reference yield: 36.0%

6-<(2E)-4-chloro-3-methylbut-2-enyl>-2,5-diketo-4-(4-methoxybenzyl)-3-benzyl-1,4-diazabicyclo<4.3.0>nonane (124268-80-0) → 2,8-diketo-9-(4-methoxybenzyl)-10-(1-methylethenyl)-1-benzyl-3,9-diazatricyclo<5.2.2.03,7>undecane (124375-85-5) + (1R,7R,11R)-7-Benzyl-11-isopropenyl-8-(4-methoxy-benzyl)-5,8-diaza-tricyclo[5.2.2.01,5]undecane-6,9-dione (124268-81-1,124375-85-5)

Guidance literature:

With sodium hydride; In hexane; N,N-dimethyl-formamide; Ambient temperature;

Reference yield:

3-Benzyl-8a-((E)-4-hydroxy-3-methyl-but-2-enyl)-2-(4-methoxy-benzyl)-hexahydro-pyrrolo[1,2-a]pyrazine-1,4-dione (124268-79-7) → (1R,7R,11R)-7-Benzyl-11-isopropenyl-8-(4-methoxy-benzyl)-5,8-diaza-tricyclo[5.2.2.01,5]undecane-6,9-dione (124268-81-1,124375-85-5)

Guidance literature:

Multi-step reaction with 2 steps

1: collidine, LiCl, methanesulfonyl chloride / dimethylformamide / Ambient temperature

2: 36 percent / NaH / dimethylformamide; hexane / Ambient temperature

With 2,3,5-trimethyl-pyridine; sodium hydride; methanesulfonyl chloride; lithium chloride; In hexane; N,N-dimethyl-formamide;

upstream raw materials:

6-<(2E)-4-chloro-3-methylbut-2-enyl>-2,5-diketo-4-(4-methoxybenzyl)-3-benzyl-1,4-diazabicyclo<4.3.0>nonane

2,8-diketo-10-(1-methylethenyl)-9-(4-methoxybenzyl)-3,9-diazatricyclo<5.2.2.0^3,7>undecane

benzyl bromide

3-Benzyl-8a-((E)-4-hydroxy-3-methyl-but-2-enyl)-2-(4-methoxy-benzyl)-hexahydro-pyrrolo[1,2-a]pyrazine-1,4-dione

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