Acrylic acid 16-iodo-hexadecyl ester

Base Information

• Chemical Name: Acrylic acid 16-iodo-hexadecyl ester
• CAS No.: 109182-99-2
• Molecular Formula: C₁₉H₃₅IO₂
• Molecular Weight: 422.39
• Mol file: 109182-99-2.mol

Synonyms:Acrylic acid 16-iodo-hexadecyl ester

Chemical Property of Acrylic acid 16-iodo-hexadecyl ester

Chemical Property:

Purity/Quality:

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Technology Process of Acrylic acid 16-iodo-hexadecyl ester

There total 1 articles about Acrylic acid 16-iodo-hexadecyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

16-bromohexadecan-1-ol (59101-28-9) → Acrylic acid 16-iodo-hexadecyl ester (109182-99-2)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine / CH₂Cl₂ / Ambient temperature

2: sodium iodide / butan-2-one / 3 h / Heating

With triethylamine; sodium iodide; In dichloromethane; butanone;

DOI:10.1021/ja00250a036

Reference yield: 56.0%

Acrylic acid 16-iodo-hexadecyl ester (109182-99-2) → hexadecyl acrylate (13402-02-3,25986-78-1) + oxacycloeicosan-2-one (58296-53-0)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tertbutyltin hydride; In benzene; for 3h; Heating;

DOI:10.1021/ja00250a036

upstream raw materials:

16-bromohexadecan-1-ol

Downstream raw materials:

hexadecyl acrylate

oxacycloeicosan-2-one