N-methyl-N-<(1S)-1-phenyl-2-(1-pyrrolidinyl)ethyl>-3-aminophenylacetamide

Base Information

Chemical Name:N-methyl-N-<(1S)-1-phenyl-2-(1-pyrrolidinyl)ethyl>-3-aminophenylacetamide
CAS No.:157947-89-2
Molecular Formula:C₂₁H₂₇N₃O
Molecular Weight:337.465
Hs Code.:

Synonyms:N-methyl-N-<(1S)-1-phenyl-2-(1-pyrrolidinyl)ethyl>-3-aminophenylacetamide

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Chemical Property of N-methyl-N-<(1S)-1-phenyl-2-(1-pyrrolidinyl)ethyl>-3-aminophenylacetamide

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Technology Process of N-methyl-N-<(1S)-1-phenyl-2-(1-pyrrolidinyl)ethyl>-3-aminophenylacetamide

There total 3 articles about N-methyl-N-<(1S)-1-phenyl-2-(1-pyrrolidinyl)ethyl>-3-aminophenylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 116508-31-7
N-methyl-N-<(1S)-1-phenyl-2-(1-pyrrolidinyl)ethyl>-3-nitrophenylacetamide

: 157947-89-2
N-methyl-N-<(1S)-1-phenyl-2-(1-pyrrolidinyl)ethyl>-3-aminophenylacetamide

Guidance literature:: With hydrogenchloride; hydrogen; palladium on activated charcoal; In methanol; for 8h; under 2327.2 Torr;
DOI:10.1021/jm00044a006

Reference yield:

: 1877-73-2
3-nitro-benzeneacetic acid

: 157947-89-2
N-methyl-N-<(1S)-1-phenyl-2-(1-pyrrolidinyl)ethyl>-3-aminophenylacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) DCC, pyridine / 1.) CH₂Cl₂, 25 deg C, 2 min, 2.) CH₂Cl₂, 12 h

2: 78 percent / H₂, 15percent aq. HCl / 5percent Pd/C / methanol / 8 h / 2327.2 Torr

With pyridine; hydrogenchloride; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol;
DOI:10.1021/jm00044a006

Reference yield:

: 116508-51-1
(1S)-N-methyl-1-phenyl-2-(pyrrolidin-1-yl)ethanamine

: 157947-89-2
N-methyl-N-<(1S)-1-phenyl-2-(1-pyrrolidinyl)ethyl>-3-aminophenylacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) DCC, pyridine / 1.) CH₂Cl₂, 25 deg C, 2 min, 2.) CH₂Cl₂, 12 h

2: 78 percent / H₂, 15percent aq. HCl / 5percent Pd/C / methanol / 8 h / 2327.2 Torr

With pyridine; hydrogenchloride; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol;
DOI:10.1021/jm00044a006