tert-butyl allyl(6-(N,N-dibenzylsulfamoyl)-1-iodonaphthalen-2-yl)carbamate

Base Information

Chemical Name:tert-butyl allyl(6-(N,N-dibenzylsulfamoyl)-1-iodonaphthalen-2-yl)carbamate
CAS No.:1363480-16-3
Molecular Formula:C₃₂H₃₃IN₂O₄S
Molecular Weight:668.596
Hs Code.:

Synonyms:tert-butyl allyl(6-(N,N-dibenzylsulfamoyl)-1-iodonaphthalen-2-yl)carbamate

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Chemical Property of tert-butyl allyl(6-(N,N-dibenzylsulfamoyl)-1-iodonaphthalen-2-yl)carbamate

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Technology Process of tert-butyl allyl(6-(N,N-dibenzylsulfamoyl)-1-iodonaphthalen-2-yl)carbamate

There total 6 articles about tert-butyl allyl(6-(N,N-dibenzylsulfamoyl)-1-iodonaphthalen-2-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1363480-14-1
tert-butyl (6-(N,N-dibenzylsulfamoyl)-1-iodonaphthalen-2-yl)carbamate

: 106-95-6
allyl bromide

: 1363480-16-3
tert-butyl allyl(6-(N,N-dibenzylsulfamoyl)-1-iodonaphthalen-2-yl)carbamate

Guidance literature:: With sodium hydride; In mineral oil; at 0 - 20 ℃; for 2.75h;
DOI:10.1021/jm201717y

Reference yield:

: 1363480-10-7
6-(N,N-dibenzylsulfamoyl)-2-naphthoic acid

: 1363480-16-3
tert-butyl allyl(6-(N,N-dibenzylsulfamoyl)-1-iodonaphthalen-2-yl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: diphenylphosphoranyl azide; triethylamine / 17 h / Reflux

2: N-iodo-succinimide; toluene-4-sulfonic acid / dichloromethane; acetonitrile / 144 h / 20 °C / Darkness

3: sodium hydride / mineral oil / 2.75 h / 0 - 20 °C

With N-iodo-succinimide; diphenylphosphoranyl azide; sodium hydride; toluene-4-sulfonic acid; triethylamine; In dichloromethane; acetonitrile; mineral oil; 1: Curtius reaction;
DOI:10.1021/jm201717y

Reference yield:

: 1363480-12-9
tert-butyl (6-(N,N-dibenzylsulfamoyl)naphthalen-2-yl)carbamate

: 1363480-16-3
tert-butyl allyl(6-(N,N-dibenzylsulfamoyl)-1-iodonaphthalen-2-yl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: N-iodo-succinimide; toluene-4-sulfonic acid / dichloromethane; acetonitrile / 144 h / 20 °C / Darkness

2: sodium hydride / mineral oil / 2.75 h / 0 - 20 °C

With N-iodo-succinimide; sodium hydride; toluene-4-sulfonic acid; In dichloromethane; acetonitrile; mineral oil;
DOI:10.1021/jm201717y