bis(ethylene acetal) of 3,5-diacetyl-1-(3,5-di-O-benzoyl-β-D-ribofuranosyl)pyridinium chloride

Base Information

Chemical Name:bis(ethylene acetal) of 3,5-diacetyl-1-(3,5-di-O-benzoyl-β-D-ribofuranosyl)pyridinium chloride
CAS No.:73591-86-3
Molecular Formula:C₃₂H₃₄NO₁₀*Cl
Molecular Weight:628.076
Hs Code.:

Synonyms:bis(ethylene acetal) of 3,5-diacetyl-1-(3,5-di-O-benzoyl-β-D-ribofuranosyl)pyridinium chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(ethylene acetal) of 3,5-diacetyl-1-(3,5-di-O-benzoyl-β-D-ribofuranosyl)pyridinium chloride

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Technology Process of bis(ethylene acetal) of 3,5-diacetyl-1-(3,5-di-O-benzoyl-β-D-ribofuranosyl)pyridinium chloride

There total 2 articles about bis(ethylene acetal) of 3,5-diacetyl-1-(3,5-di-O-benzoyl-β-D-ribofuranosyl)pyridinium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 73611-06-0
3,5-di-O-benzoyl-β-D-ribofuranosyl chloride

: 73591-73-8
3,5-diacetylpyridine bis(ethylene acetal)

: 73591-86-3
bis(ethylene acetal) of 3,5-diacetyl-1-(3,5-di-O-benzoyl-β-D-ribofuranosyl)pyridinium chloride

Guidance literature:: In acetonitrile; at -5 ℃; for 72h;
DOI:10.1016/0008-6215(80)90003-8

Reference yield:

: 1199-61-7
2,6-diacetylpyridine

: 73591-86-3
bis(ethylene acetal) of 3,5-diacetyl-1-(3,5-di-O-benzoyl-β-D-ribofuranosyl)pyridinium chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / conc. H₂SO₄ / benzene / Heating

2: 75 percent / acetonitrile / 72 h / -5 °C

With sulfuric acid; In acetonitrile; benzene;
DOI:10.1016/0008-6215(80)90003-8