4-chlorophenelzine

Base Information

• Chemical Name: 4-chlorophenelzine
• CAS No.: 25198-48-5
• Molecular Formula: C8H11 Cl N2
• Molecular Weight: 170.642
• Hs Code.: 2928000090
• Mol file: 25198-48-5.mol

Synonyms:Hydrazine,(p-chlorophenethyl)- (7CI,8CI); p-Chlorophenethylhydrazine

Chemical Property of 4-chlorophenelzine

Chemical Property:

• Vapor Pressure: 0.000452mmHg at 25°C
• Refractive Index: 1.565
• Boiling Point: 314.9°Cat760mmHg
• PKA: 8.04±0.70(Predicted)
• Flash Point: 144.3°C
• PSA: 38.05000
• Density: 1.163g/cm³
• LogP: 2.43700

Purity/Quality:

2-(4-chlorophenyl)ethylhydrazine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-chlorophenelzine

There total 2 articles about 4-chlorophenelzine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-chloro-4-(2-chloroethyl)benzene (32327-70-1) → 4-Chlor-phenethyl-hydrazin (25198-48-5)

Guidance literature:

With hydrazine hydrate; In isopropyl alcohol; Heating;

Reference yield:

2-(4-Chlorophenyl)ethanol (1875-88-3) → 4-Chlor-phenethyl-hydrazin (25198-48-5)

Guidance literature:

Multistep reaction; (i) SOCl₂, benzene, (ii) N₂H₄*H₂O, nPrOH;

DOI:10.1021/jm00300a007

Reference yield: 42.0%

2-oxo-propionic acid (127-17-3) + 4-Chlor-phenethyl-hydrazin (25198-48-5) → 2-{[2-(4-Chloro-phenyl)-ethyl]-hydrazono}-propionic acid (69717-66-4)

Guidance literature:

With sodium acetate; In water; for 2h;

DOI:10.1021/jm00148a011

upstream raw materials:

2-(4-Chlorophenyl)ethanol

1-chloro-4-(2-chloroethyl)benzene

Downstream raw materials:

β-(p-Chlorphenyl)-ethylaminoguanidin

N-Amino-N-4-chlorphenethylguanidin

2-{[2-(4-Chloro-phenyl)-ethyl]-hydrazono}-propionic acid

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