C₂₅H₃₁NO₁₃

Base Information

Chemical Name:C₂₅H₃₁NO₁₃
CAS No.:1360926-33-5
Molecular Formula:C₂₅H₃₁NO₁₃
Molecular Weight:553.52
Hs Code.:

C<sub>25</sub>H<sub>31</sub>NO<sub>13</sub>

Synonyms:C₂₅H₃₁NO₁₃

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Chemical Property of C₂₅H₃₁NO₁₃

Chemical Property:

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Technology Process of C₂₅H₃₁NO₁₃

There total 5 articles about C₂₅H₃₁NO₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 32315-10-9
bis(trichloromethyl) carbonate

: 1242935-03-0
C₂₄H₃₃NO₁₂

: 1360926-33-5
C₂₅H₃₁NO₁₃

Guidance literature:: With triethylamine; In 1,2-dichloro-ethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1039/c1cc13826j

Reference yield:

: 604-68-2
α-D-glucopyranose peracetylate

: 1360926-33-5
C₂₅H₃₁NO₁₃

Guidance literature:: Multi-step reaction with 6 steps

1: methanol; Acetyl bromide / acetic acid / 24 h / 20 °C / Inert atmosphere

2: sodium sulfate; silver carbonate / dichloromethane / 36 h / 20 °C / Inert atmosphere

3: dmap; triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

4: potassium carbonate / N,N-dimethyl-formamide / 20 - 90 °C / Inert atmosphere

5: palladium 10% on activated carbon; hydrogen / ethyl acetate / 5 h / 20 °C

6: triethylamine / 1,2-dichloro-ethane / 0 - 20 °C / Inert atmosphere

With methanol; dmap; Acetyl bromide; palladium 10% on activated carbon; hydrogen; potassium carbonate; sodium sulfate; triethylamine; silver carbonate; In dichloromethane; acetic acid; ethyl acetate; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1039/c1cc13826j

Reference yield:

: 126765-18-2
2-[(2-hydroxyethyl)oxy]ethyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

: 1360926-33-5
C₂₅H₃₁NO₁₃

Guidance literature:: Multi-step reaction with 4 steps

1: dmap; triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

2: potassium carbonate / N,N-dimethyl-formamide / 20 - 90 °C / Inert atmosphere

3: palladium 10% on activated carbon; hydrogen / ethyl acetate / 5 h / 20 °C

4: triethylamine / 1,2-dichloro-ethane / 0 - 20 °C / Inert atmosphere

With dmap; palladium 10% on activated carbon; hydrogen; potassium carbonate; triethylamine; In dichloromethane; ethyl acetate; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1039/c1cc13826j