(3S,6S)-3-allyl-1-(2,4-dimethoxybenzyl)-4-iodo-6-methyl-3,6-dihydro-1H-pyridin-2-one

Base Information

Chemical Name:(3S,6S)-3-allyl-1-(2,4-dimethoxybenzyl)-4-iodo-6-methyl-3,6-dihydro-1H-pyridin-2-one
CAS No.:898831-88-4
Molecular Formula:C₁₈H₂₂INO₃
Molecular Weight:427.282
Hs Code.:

Synonyms:(3S,6S)-3-allyl-1-(2,4-dimethoxybenzyl)-4-iodo-6-methyl-3,6-dihydro-1H-pyridin-2-one

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Chemical Property of (3S,6S)-3-allyl-1-(2,4-dimethoxybenzyl)-4-iodo-6-methyl-3,6-dihydro-1H-pyridin-2-one

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Technology Process of (3S,6S)-3-allyl-1-(2,4-dimethoxybenzyl)-4-iodo-6-methyl-3,6-dihydro-1H-pyridin-2-one

There total 13 articles about (3S,6S)-3-allyl-1-(2,4-dimethoxybenzyl)-4-iodo-6-methyl-3,6-dihydro-1H-pyridin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.9%

: 898831-93-1
(3S,6S)-1-(2,4-dimethoxybenzyl)-4-iodo-6-methyl-3-[3-(2-nitrophenylselanyl)propyl]-3,6-dihydro-1H-pyridin-2-one

: 898831-88-4
(3S,6S)-3-allyl-1-(2,4-dimethoxybenzyl)-4-iodo-6-methyl-3,6-dihydro-1H-pyridin-2-one

Guidance literature:: With dihydrogen peroxide; In tetrahydrofuran; at 20 ℃; for 3h;
DOI:10.1021/jo0606002

Reference yield: 92.0%

: 898831-77-1
(5S,6S)-1-(2,4-dimethoxybenzyl)-5-diphenylphosphoryloxy-4-iodo-6-methyl-5,6-dihydro-1H-pyridin-2-one

: 72824-04-5
2-Allyl-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 898831-88-4
(3S,6S)-3-allyl-1-(2,4-dimethoxybenzyl)-4-iodo-6-methyl-3,6-dihydro-1H-pyridin-2-one

: 5-allyl-1-(2,4-dimethoxy-benzyl)-4-iodo-6-methyl-5,6-dihydro-1H-pyridin-2-one

Guidance literature:: With lithium isopropoxide; In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.1016/j.tetlet.2007.03.017

Reference yield: 22.0%

: 898831-77-1
(5S,6S)-1-(2,4-dimethoxybenzyl)-5-diphenylphosphoryloxy-4-iodo-6-methyl-5,6-dihydro-1H-pyridin-2-one

: 2622-05-1
allylmagnesium bromide

: (6S)-1-(2,4-dimethoxybenzyl)-4-iodo-6-methyl-3,6-dihydro-1H-pyridin-2-one

: 898831-88-4
(3S,6S)-3-allyl-1-(2,4-dimethoxybenzyl)-4-iodo-6-methyl-3,6-dihydro-1H-pyridin-2-one

: 5-allyl-1-(2,4-dimethoxy-benzyl)-4-iodo-6-methyl-5,6-dihydro-1H-pyridin-2-one

Guidance literature:: allylmagnesium bromide; With lithium chloride; zinc(II) chloride; In tetrahydrofuran; at -78 - 0 ℃; for 0.0833333h;

(5S,6S)-1-(2,4-dimethoxybenzyl)-5-diphenylphosphoryloxy-4-iodo-6-methyl-5,6-dihydro-1H-pyridin-2-one; In tetrahydrofuran; at -78 - 0 ℃; for 0.666667h;
DOI:10.1016/j.tetlet.2007.03.017