(S)-2-(2,3-Dimethoxy-benzoylamino)-pentanedioic acid 5-amide 1-(2,3-dimethoxy-benzylamide)

Base Information

Chemical Name:(S)-2-(2,3-Dimethoxy-benzoylamino)-pentanedioic acid 5-amide 1-(2,3-dimethoxy-benzylamide)
CAS No.:857064-54-1
Molecular Formula:C₂₃H₂₉N₃O₇
Molecular Weight:459.499
Hs Code.:

Synonyms:(S)-2-(2,3-Dimethoxy-benzoylamino)-pentanedioic acid 5-amide 1-(2,3-dimethoxy-benzylamide)

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Chemical Property of (S)-2-(2,3-Dimethoxy-benzoylamino)-pentanedioic acid 5-amide 1-(2,3-dimethoxy-benzylamide)

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Technology Process of (S)-2-(2,3-Dimethoxy-benzoylamino)-pentanedioic acid 5-amide 1-(2,3-dimethoxy-benzylamide)

There total 4 articles about (S)-2-(2,3-Dimethoxy-benzoylamino)-pentanedioic acid 5-amide 1-(2,3-dimethoxy-benzylamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 857064-49-4
(S)-2-Amino-pentanedioic acid 5-amide 1-(2,3-dimethoxy-benzylamide)

: 1521-38-6
2,3-dimethoxybenzoic acid

: 857064-54-1
(S)-2-(2,3-Dimethoxy-benzoylamino)-pentanedioic acid 5-amide 1-(2,3-dimethoxy-benzylamide)

Guidance literature:: 2,3-dimethoxybenzoic acid; With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In acetonitrile; at 20 ℃; for 0.333333h;

(S)-2-Amino-pentanedioic acid 5-amide 1-(2,3-dimethoxy-benzylamide); In acetonitrile; at 20 ℃; for 96h;
DOI:10.1055/s-2005-861865

Reference yield:

: 857064-45-0
[3-carbamoyl-1-(2,3-dimethoxy-benzylcarbamoyl)-propyl]-carbamic acid 9H-fluoren-9-ylmethyl ester

: 857064-54-1
(S)-2-(2,3-Dimethoxy-benzoylamino)-pentanedioic acid 5-amide 1-(2,3-dimethoxy-benzylamide)

Guidance literature:: Multi-step reaction with 2 steps

1.1: 100 percent / piperidine / acetonitrile / 24 h / 20 °C

2.1: HBTU; (i-Pr)2NEt / acetonitrile / 0.33 h / 20 °C

2.2: 88 percent / acetonitrile / 96 h / 20 °C

With piperidine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In acetonitrile;
DOI:10.1055/s-2005-861865

Reference yield:

: 4393-09-3
2,3-dimethoxybenzyl amine

: 857064-54-1
(S)-2-(2,3-Dimethoxy-benzoylamino)-pentanedioic acid 5-amide 1-(2,3-dimethoxy-benzylamide)

Guidance literature:: Multi-step reaction with 3 steps

1.1: HBTU; (i-Pr)2NEt / acetonitrile / 0.33 h / 20 °C

1.2: 87 percent / acetonitrile / 20 °C

2.1: 100 percent / piperidine / acetonitrile / 24 h / 20 °C

3.1: HBTU; (i-Pr)2NEt / acetonitrile / 0.33 h / 20 °C

3.2: 88 percent / acetonitrile / 96 h / 20 °C

With piperidine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In acetonitrile;
DOI:10.1055/s-2005-861865