(3S,4S)-4-isobutylpyrrolidine-1,3-dicarboxylic acid 1-benzyl ester 3-methyl ester

Base Information

Chemical Name:(3S,4S)-4-isobutylpyrrolidine-1,3-dicarboxylic acid 1-benzyl ester 3-methyl ester
CAS No.:1009643-84-8
Molecular Formula:C₁₈H₂₅NO₄
Molecular Weight:319.401
Hs Code.:

Synonyms:(3S,4S)-4-isobutylpyrrolidine-1,3-dicarboxylic acid 1-benzyl ester 3-methyl ester

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Chemical Property of (3S,4S)-4-isobutylpyrrolidine-1,3-dicarboxylic acid 1-benzyl ester 3-methyl ester

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Technology Process of (3S,4S)-4-isobutylpyrrolidine-1,3-dicarboxylic acid 1-benzyl ester 3-methyl ester

There total 1 articles about (3S,4S)-4-isobutylpyrrolidine-1,3-dicarboxylic acid 1-benzyl ester 3-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 52745-92-3
methyl (E)-3-nitroacrylate

: 1119-16-0
isocaproic aldehyde

: 501-53-1,94274-21-2
benzyl chloroformate

: 1009643-84-8
(3S,4S)-4-isobutylpyrrolidine-1,3-dicarboxylic acid 1-benzyl ester 3-methyl ester

Guidance literature:: methyl (E)-3-nitroacrylate; isocaproic aldehyde; With benzoic acid; In water; at 0 - 20 ℃;

With hydrogen; palladium dihydroxide; In methanol; for 24h; under 3800.26 Torr;

benzyl chloroformate; With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃; Further stages.;
DOI:10.1002/anie.200704161

Reference yield: 90.0%

: 1009643-84-8
(3S,4S)-4-isobutylpyrrolidine-1,3-dicarboxylic acid 1-benzyl ester 3-methyl ester

: 261896-39-3
(3S,4S)-4-(2'-methylprop-1'-yl)-3-pyrrolidine carboxylic acid

Guidance literature:: (3S,4S)-4-isobutylpyrrolidine-1,3-dicarboxylic acid 1-benzyl ester 3-methyl ester; With lithium hydroxide; In tetrahydrofuran; methanol; water; at 0 ℃; for 1.5h;

With hydrogen; palladium on activated charcoal; In methanol; for 6h; under 760.051 Torr; Further stages.;
DOI:10.1002/anie.200704161