(S)-4-[(S)-1-Azidocarbonyl-2-(1H-imidazol-4-yl)-ethylcarbamoyl]-4-benzyloxycarbonylamino-butyric acid tert-butyl ester

Base Information

• Chemical Name: (S)-4-[(S)-1-Azidocarbonyl-2-(1H-imidazol-4-yl)-ethylcarbamoyl]-4-benzyloxycarbonylamino-butyric acid tert-butyl ester
• CAS No.: 51221-20-6
• Molecular Formula: C₂₃H₂₉N₇O₆
• Molecular Weight: 499.527

Synonyms:(S)-4-[(S)-1-Azidocarbonyl-2-(1H-imidazol-4-yl)-ethylcarbamoyl]-4-benzyloxycarbonylamino-butyric acid tert-butyl ester

Chemical Property of (S)-4-[(S)-1-Azidocarbonyl-2-(1H-imidazol-4-yl)-ethylcarbamoyl]-4-benzyloxycarbonylamino-butyric acid tert-butyl ester

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Technology Process of (S)-4-[(S)-1-Azidocarbonyl-2-(1H-imidazol-4-yl)-ethylcarbamoyl]-4-benzyloxycarbonylamino-butyric acid tert-butyl ester

There total 1 articles about (S)-4-[(S)-1-Azidocarbonyl-2-(1H-imidazol-4-yl)-ethylcarbamoyl]-4-benzyloxycarbonylamino-butyric acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-Z-γ-tert-butylglutamyl-histidine hydrazide (3979-08-6) → (S)-4-[(S)-1-Azidocarbonyl-2-(1H-imidazol-4-yl)-ethylcarbamoyl]-4-benzyloxycarbonylamino-butyric acid tert-butyl ester (51221-20-6)

Guidance literature:

With hydrogenchloride; sodium nitrite; In water; N,N-dimethyl-formamide; at 0 ℃; for 0.0666667h;

Reference yield: 70.0%

(S)-4-[(S)-1-Azidocarbonyl-2-(1H-imidazol-4-yl)-ethylcarbamoyl]-4-benzyloxycarbonylamino-butyric acid tert-butyl ester (51221-20-6) + L-sarcolysyl-Nω-nitroarginyl-tryptophyl-glycine methyl ester hydrochloride → N-Z-γ-tert-butylglutamyl-histidyl-L-sarcolysyl-Nω-nitroarginyl-tryptophyl-glycine methyl ester (85642-52-0)

Guidance literature:

With triethylamine; In ethyl acetate; N,N-dimethyl-formamide; at 4 ℃; for 48h;

Reference yield: 69.0%

(S)-4-[(S)-1-Azidocarbonyl-2-(1H-imidazol-4-yl)-ethylcarbamoyl]-4-benzyloxycarbonylamino-butyric acid tert-butyl ester (51221-20-6) + D-sarcolysyl-Nω-nitroarginyl-tryptophyl-glycine methyl ester hydrochloride → N-Z-γ-tert-butylglutamyl-histidyl-D-sarcolysyl-Nω-nitroarginyl-tryptophyl-glycine methyl ester (85642-53-1)

Guidance literature:

With triethylamine; In ethyl acetate; N,N-dimethyl-formamide; at 4 ℃; for 48h;

upstream raw materials:

N-Z-γ-tert-butylglutamyl-histidine hydrazide

Downstream raw materials:

N-Z-γ-tert-butylglutamyl-histidyl-D-sarcolysyl-N^ω-nitroarginyl-tryptophyl-glycine methyl ester

N-Z-γ-tert-butylglutamyl-histidyl-L-sarcolysyl-N^ω-nitroarginyl-tryptophyl-glycine methyl ester

N-Z-γ-tert-butylglutamyl-histidyl-D-sarcolysyl-N^ε-Z-lysyl-tryptophyl-glycine methyl ester

N-Z-γ-tert-butylglutamyl-histidyl-L-sarcolysyl-N^ε-Z-lysyl-tryptophyl-glycine methyl ester

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