1-(triphenylphosphino)-1H-cyclobutanaphthalene bromide

Base Information

Chemical Name:1-(triphenylphosphino)-1H-cyclobutanaphthalene bromide
CAS No.:85924-89-6
Molecular Formula:C₂₉H₂₂BrP
Molecular Weight:481.371
Hs Code.:

1-(triphenylphosphino)-1H-cyclobuta<de>naphthalene bromide

Synonyms:1-(triphenylphosphino)-1H-cyclobutanaphthalene bromide

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Chemical Property of 1-(triphenylphosphino)-1H-cyclobutanaphthalene bromide

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Technology Process of 1-(triphenylphosphino)-1H-cyclobutanaphthalene bromide

There total 4 articles about 1-(triphenylphosphino)-1H-cyclobutanaphthalene bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 54125-11-0
1-Bromo-1H-cyclobutanaphthalene

: 603-35-0
triphenylphosphine

: 85924-89-6
1-(triphenylphosphino)-1H-cyclobutanaphthalene bromide

Guidance literature:: In xylene; for 72h; Heating;
DOI:10.1021/ja00357a022

Reference yield:

: 24973-91-9
1H-Cyclobutanaphthalene

: 85924-89-6
1-(triphenylphosphino)-1H-cyclobutanaphthalene bromide

Guidance literature:: Multi-step reaction with 2 steps

1: 40 percent / N-bromosuccinimide, benzoyl peroxide / CCl₄ / 4.5 h / Heating

2: 97 percent / xylene / 72 h / Heating

With N-Bromosuccinimide; Perbenzoic acid; In tetrachloromethane; xylene;
DOI:10.1021/ja00357a022

Reference yield:

: 85924-73-8
C₁₁H₇Li

: 85924-89-6
1-(triphenylphosphino)-1H-cyclobutanaphthalene bromide

Guidance literature:: Multi-step reaction with 3 steps

1: 25 mg / tetrahydrofuran / 0.17 h / -78 °C

2: 40 percent / N-bromosuccinimide, benzoyl peroxide / CCl₄ / 4.5 h / Heating

3: 97 percent / xylene / 72 h / Heating

With N-Bromosuccinimide; Perbenzoic acid; In tetrahydrofuran; tetrachloromethane; xylene;
DOI:10.1021/ja00357a022