C₁₆H₁₂ClNO₃

Base Information

Chemical Name:C₁₆H₁₂ClNO₃
CAS No.:1588471-65-1
Molecular Formula:C₁₆H₁₂ClNO₃
Molecular Weight:301.729
Hs Code.:

C<sub>16</sub>H<sub>12</sub>ClNO<sub>3</sub>

Synonyms:C₁₆H₁₂ClNO₃

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Chemical Property of C₁₆H₁₂ClNO₃

Chemical Property:

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Technology Process of C₁₆H₁₂ClNO₃

There total 4 articles about C₁₆H₁₂ClNO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1588471-62-8
C₁₆H₁₃NO₄

: 1588471-65-1
C₁₆H₁₂ClNO₃

Guidance literature:: With sulfuryl dichloride; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1021/ol5007339

Reference yield:

: 85-44-9
phthalic anhydride

: 1588471-65-1
C₁₆H₁₂ClNO₃

Guidance literature:: Multi-step reaction with 4 steps

1: acetic acid / 5 h / 110 °C

2: trifluoroacetic acid; hydrogenchloride / 20 h / 74 °C / Inert atmosphere; Reflux

3: zinc(II) chloride; sodium cyanoborohydride / methanol / 12 h / 20 °C / Inert atmosphere

4: sulfuryl dichloride / dichloromethane / 20 °C / Inert atmosphere

With hydrogenchloride; sulfuryl dichloride; sodium cyanoborohydride; trifluoroacetic acid; zinc(II) chloride; In methanol; dichloromethane; acetic acid;
DOI:10.1021/ol5007339

Reference yield:

: 491875-12-8
C₁₅H₁₁NO₃

: 1588471-65-1
C₁₆H₁₂ClNO₃

Guidance literature:: Multi-step reaction with 3 steps

1: trifluoroacetic acid; hydrogenchloride / 20 h / 74 °C / Inert atmosphere; Reflux

2: zinc(II) chloride; sodium cyanoborohydride / methanol / 12 h / 20 °C / Inert atmosphere

3: sulfuryl dichloride / dichloromethane / 20 °C / Inert atmosphere

With hydrogenchloride; sulfuryl dichloride; sodium cyanoborohydride; trifluoroacetic acid; zinc(II) chloride; In methanol; dichloromethane;
DOI:10.1021/ol5007339