C₂₃H₃₀N₂O₁₀

Base Information

• Chemical Name: C₂₃H₃₀N₂O₁₀
• CAS No.: 1383117-23-4
• Molecular Formula: C₂₃H₃₀N₂O₁₀
• Molecular Weight: 494.499
• Mol file: 1383117-23-4.mol

Synonyms:C₂₃H₃₀N₂O₁₀

Chemical Property of C₂₃H₃₀N₂O₁₀

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₃H₃₀N₂O₁₀

There total 5 articles about C₂₃H₃₀N₂O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C37H40N2O10 → C23H30N2O10 (1383117-23-4)

Guidance literature:

With 5%-palladium/activated carbon; hydrogen; In ethyl acetate; at 20 ℃; for 8h; under 38787.1 Torr;

DOI:10.1021/ja408034x

Reference yield:

C10H14N2O5 → C23H30N2O10 (1383117-23-4)

Guidance literature:

Multi-step reaction with 3 steps

1.1: potassium tert-butylate / tetrahydrofuran; tert-butyl alcohol / 0.67 h / -78 - 0 °C

1.2: 0.17 h / 0 °C

2.1: dmap / tetrahydrofuran / 3.5 h / 20 °C

3.1: 5%-palladium/activated carbon; hydrogen / ethyl acetate / 8 h / 20 °C / 38787.1 Torr

With dmap; 5%-palladium/activated carbon; potassium tert-butylate; hydrogen; In tetrahydrofuran; ethyl acetate; tert-butyl alcohol;

DOI:10.1021/ja408034x

Reference yield:

dimethyl (S)-3-(3,6-dioxopiperazin-2-yl)propionate (433285-16-6) → C23H30N2O10 (1383117-23-4)

Guidance literature:

Multi-step reaction with 4 steps

1.1: 18 h / 130 °C

2.1: potassium tert-butylate / tetrahydrofuran; tert-butyl alcohol / 0.67 h / -78 - 0 °C

2.2: 0.17 h / 0 °C

3.1: dmap / tetrahydrofuran / 3.5 h / 20 °C

4.1: 5%-palladium/activated carbon; hydrogen / ethyl acetate / 8 h / 20 °C / 38787.1 Torr

With dmap; 5%-palladium/activated carbon; potassium tert-butylate; hydrogen; In tetrahydrofuran; ethyl acetate; tert-butyl alcohol;

DOI:10.1021/ja408034x

upstream raw materials:

dimethyl (S)-3-(3,6-dioxopiperazin-2-yl)propionate

C₁₂H₁₆N₂O₆

Downstream raw materials:

C₃₅H₃₆N₂O₉

C₃₅H₃₈N₂O₁₁

C₃₅H₃₈N₂O₁₂

C₂₁H₃₀N₂O₉