N,N-dimethyl-(2-benzyl-4,4-dimethyl-1-cyclohexenyl)methylamine hydrochloride

Base Information

Chemical Name:N,N-dimethyl-(2-benzyl-4,4-dimethyl-1-cyclohexenyl)methylamine hydrochloride
CAS No.:64969-91-1
Molecular Formula:C₁₈H₂₇N*ClH
Molecular Weight:293.88
Hs Code.:

Synonyms:N,N-dimethyl-(2-benzyl-4,4-dimethyl-1-cyclohexenyl)methylamine hydrochloride

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Chemical Property of N,N-dimethyl-(2-benzyl-4,4-dimethyl-1-cyclohexenyl)methylamine hydrochloride

Chemical Property:

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Technology Process of N,N-dimethyl-(2-benzyl-4,4-dimethyl-1-cyclohexenyl)methylamine hydrochloride

There total 3 articles about N,N-dimethyl-(2-benzyl-4,4-dimethyl-1-cyclohexenyl)methylamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.0%

: 63347-26-2,90546-92-2
1-benzyl-c-2-dimethylaminomethyl-5,5-dimethyl-r-1-cyclohexanol

: 64969-90-0
N,N-dimethyl-(2-benzyl-4,4-dimethyl-2-cyclohexenyl)methylamine hydrochloride

: 64969-91-1
N,N-dimethyl-(2-benzyl-4,4-dimethyl-1-cyclohexenyl)methylamine hydrochloride

Guidance literature:: With hydrogenchloride; phosphorus tribromide; 1) C₆H₆, 4 h, 0-5 deg C; 2) EtOH;
DOI:10.1248/cpb.32.44

Reference yield:

: 100-44-7
benzyl chloride

: 64969-91-1
N,N-dimethyl-(2-benzyl-4,4-dimethyl-1-cyclohexenyl)methylamine hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 60.5 g / Mg / diethyl ether / 4 h / Heating

2: 2.2 percent / 1) PBr₃; 2) conc. HCl / benzene; diethyl ether / 4 h / 0 - 5 °C

With hydrogenchloride; phosphorus tribromide; magnesium; In diethyl ether; benzene;
DOI:10.1248/cpb.32.44

Reference yield:

: 63406-25-7
5,5-dimethyl-2-(dimethylaminomethyl)cyclohexanone

: 64969-91-1
N,N-dimethyl-(2-benzyl-4,4-dimethyl-1-cyclohexenyl)methylamine hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 60.5 g / Mg / diethyl ether / 4 h / Heating

2: 2.2 percent / 1) PBr₃; 2) conc. HCl / benzene; diethyl ether / 4 h / 0 - 5 °C

With hydrogenchloride; phosphorus tribromide; magnesium; In diethyl ether; benzene;
DOI:10.1248/cpb.32.44