6-(toluene-4-sulfonylamino)methyl-1,4,5,6-tetrahydropyridine-3-carboxylic acid dimethylamide

Base Information

Chemical Name:6-(toluene-4-sulfonylamino)methyl-1,4,5,6-tetrahydropyridine-3-carboxylic acid dimethylamide
CAS No.:780785-15-1
Molecular Formula:C₁₆H₂₃N₃O₃S
Molecular Weight:337.443
Hs Code.:

Synonyms:6-(toluene-4-sulfonylamino)methyl-1,4,5,6-tetrahydropyridine-3-carboxylic acid dimethylamide

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Chemical Property of 6-(toluene-4-sulfonylamino)methyl-1,4,5,6-tetrahydropyridine-3-carboxylic acid dimethylamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of 6-(toluene-4-sulfonylamino)methyl-1,4,5,6-tetrahydropyridine-3-carboxylic acid dimethylamide

There total 4 articles about 6-(toluene-4-sulfonylamino)methyl-1,4,5,6-tetrahydropyridine-3-carboxylic acid dimethylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 780784-69-2
(S)-2-cyano-5-dimethylcarbamoyl-2H-pyridine-1-carboxylic acid methyl ester

: 780785-15-1
6-(toluene-4-sulfonylamino)methyl-1,4,5,6-tetrahydropyridine-3-carboxylic acid dimethylamide

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / Pd/C / methanol / 0.25 h / 20 °C

2: H₂; HCl / Pd/C / ethanol / 1 h / 20 °C

3: Et₃N / CH₂Cl₂ / 1 h / 20 °C

4: aq. NaOH / methanol / 1.5 h / Heating

With hydrogenchloride; sodium hydroxide; hydrogen; triethylamine; palladium on activated charcoal; In methanol; ethanol; dichloromethane;
DOI:10.1021/ja045966f

Reference yield:

: 780785-11-7
2-cyano-5-dimethylcarbamoyl-3,4-dihydro-2H-pyridine-1-carboxylic acid methyl ester

: 780785-15-1
6-(toluene-4-sulfonylamino)methyl-1,4,5,6-tetrahydropyridine-3-carboxylic acid dimethylamide

Guidance literature:: Multi-step reaction with 3 steps

1: H₂; HCl / Pd/C / ethanol / 1 h / 20 °C

2: Et₃N / CH₂Cl₂ / 1 h / 20 °C

3: aq. NaOH / methanol / 1.5 h / Heating

With hydrogenchloride; sodium hydroxide; hydrogen; triethylamine; palladium on activated charcoal; In methanol; ethanol; dichloromethane;
DOI:10.1021/ja045966f