2,2,2-trifluoroethyl {(1S)-1-methyl-2-[(4-methylbenzoyl)amino]ethyl}carbamate

Base Information

Chemical Name:2,2,2-trifluoroethyl {(1S)-1-methyl-2-[(4-methylbenzoyl)amino]ethyl}carbamate
CAS No.:951242-85-6
Molecular Formula:C₁₄H₁₇F₃N₂O₃
Molecular Weight:318.296
Hs Code.:

Synonyms:2,2,2-trifluoroethyl {(1S)-1-methyl-2-[(4-methylbenzoyl)amino]ethyl}carbamate

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Chemical Property of 2,2,2-trifluoroethyl {(1S)-1-methyl-2-[(4-methylbenzoyl)amino]ethyl}carbamate

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Technology Process of 2,2,2-trifluoroethyl {(1S)-1-methyl-2-[(4-methylbenzoyl)amino]ethyl}carbamate

There total 4 articles about 2,2,2-trifluoroethyl {(1S)-1-methyl-2-[(4-methylbenzoyl)amino]ethyl}carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 951242-84-5
(2S)-N₂-(2,2,2-trifluoroethoxycarbonyl)-1,2-propaneamine hydrochloride

: 874-60-2
4-methyl-benzoyl chloride

: 951242-85-6
2,2,2-trifluoroethyl {(1S)-1-methyl-2-[(4-methylbenzoyl)amino]ethyl}carbamate

Guidance literature:: With sodium hydrogencarbonate; In water; ethyl acetate; at 20 ℃; for 2.5h;

Reference yield: 84.0%

: 951242-85-6
2,2,2-trifluoroethyl {(1S)-1-methyl-2-[(4-methylbenzoyl)amino]ethyl}carbamate

Guidance literature:

Reference yield:

: 951242-82-3
N-(2,2,2-trifluoroethoxycarbonyl)-L-alaninamide

: 951242-85-6
2,2,2-trifluoroethyl {(1S)-1-methyl-2-[(4-methylbenzoyl)amino]ethyl}carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride / toluene; N,N-dimethyl-formamide / 2 h / 20 °C

2: 5%-palladium/activated carbon; ammonium formate; acetic acid / isopropyl alcohol / 2.5 h / 20 °C

3: sodium hydrogencarbonate / water; ethyl acetate / 2.5 h / 20 °C

With oxalyl dichloride; 5%-palladium/activated carbon; ammonium formate; sodium hydrogencarbonate; acetic acid; In water; ethyl acetate; N,N-dimethyl-formamide; isopropyl alcohol; toluene;