benzyl 4)-O-(2,3,6-trideoxy-3-trifluoroacetamido-α-L-lyxo-hexopyranosyl)-(1->4)-(2,3,6-trideoxy-3-trifluoroacetamido-α-L-lyxo-hexopyranoside)>

Base Information

Chemical Name:benzyl 4)-O-(2,3,6-trideoxy-3-trifluoroacetamido-α-L-lyxo-hexopyranosyl)-(1->4)-(2,3,6-trideoxy-3-trifluoroacetamido-α-L-lyxo-hexopyranoside)>
CAS No.:128135-63-7
Molecular Formula:C₃₃H₄₂F₆N₂O₁₂
Molecular Weight:772.693
Hs Code.:

benzyl <O-(3,4-di-O-acetyl-2,6-dideoxy-α-L-lyxo-hexopyranosyl)-(1->4)-O-(2,3,6-trideoxy-3-trifluoroacetamido-α-L-lyxo-hexopyranosyl)-(1->4)-(2,3,6-trideoxy-3-trifluoroacetamido-α-L-lyxo-hexopyranoside)>

Synonyms:benzyl 4)-O-(2,3,6-trideoxy-3-trifluoroacetamido-α-L-lyxo-hexopyranosyl)-(1->4)-(2,3,6-trideoxy-3-trifluoroacetamido-α-L-lyxo-hexopyranoside)>

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Chemical Property of benzyl 4)-O-(2,3,6-trideoxy-3-trifluoroacetamido-α-L-lyxo-hexopyranosyl)-(1->4)-(2,3,6-trideoxy-3-trifluoroacetamido-α-L-lyxo-hexopyranoside)>

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Technology Process of benzyl 4)-O-(2,3,6-trideoxy-3-trifluoroacetamido-α-L-lyxo-hexopyranosyl)-(1->4)-(2,3,6-trideoxy-3-trifluoroacetamido-α-L-lyxo-hexopyranoside)>

There total 13 articles about benzyl 4)-O-(2,3,6-trideoxy-3-trifluoroacetamido-α-L-lyxo-hexopyranosyl)-(1->4)-(2,3,6-trideoxy-3-trifluoroacetamido-α-L-lyxo-hexopyranoside)> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 128135-55-7
3,4-di-O-acetyl-1-O-tert-butyldimethylsilyl-2,6-dideoxy-β-L-lyxo-hexopyranose

: 81703-97-1
benzyl 2,3,6-trideoxy-3-trifluoroacetamido-α-L-lyxo-hexopyranoside

: 128135-62-6
benzyl 3,4-di-O-acetyl-2,6-dideoxy-α-L-lyxo-hexopyranoside

: 81661-50-9
benzyl 2,3,6-trideoxy-4-O-(3,4-di-O-acetyl-2,6-dideoxy-α-L-lyxo-hexopyranosyl)-3-trifluoroacetamido-α-L-lyxo-hexopyranoside

: 128135-63-7
benzyl 4)-O-(2,3,6-trideoxy-3-trifluoroacetamido-α-L-lyxo-hexopyranosyl)-(1->4)-(2,3,6-trideoxy-3-trifluoroacetamido-α-L-lyxo-hexopyranoside)>

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; Molekularsieb 4 Angstroem; In dichloromethane; at -50 ℃;

Reference yield:

: 128135-55-7
3,4-di-O-acetyl-1-O-tert-butyldimethylsilyl-2,6-dideoxy-β-L-lyxo-hexopyranose

: 128135-68-2
N-{(2S,3S,4S,6R)-6-Benzyloxy-3-[(2S,4S,5S,6S)-5-hydroxy-6-methyl-4-(2,2,2-trifluoro-acetylamino)-tetrahydro-pyran-2-yloxy]-2-methyl-tetrahydro-pyran-4-yl}-2,2,2-trifluoro-acetamide

: 128135-63-7
benzyl 4)-O-(2,3,6-trideoxy-3-trifluoroacetamido-α-L-lyxo-hexopyranosyl)-(1->4)-(2,3,6-trideoxy-3-trifluoroacetamido-α-L-lyxo-hexopyranoside)>

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; Molekularsieb 4 Angstroem; In dichloromethane; at -50 ℃; Yield given;

Reference yield:

: 127112-84-9,127112-87-2,132814-68-7,132814-74-5
3,4-Di-O-acetyl-2,6-dideoxy-L-lyxo-hexopyranose

: 128135-63-7
benzyl 4)-O-(2,3,6-trideoxy-3-trifluoroacetamido-α-L-lyxo-hexopyranosyl)-(1->4)-(2,3,6-trideoxy-3-trifluoroacetamido-α-L-lyxo-hexopyranoside)>

Guidance literature:: Multi-step reaction with 2 steps

1: imidazole / 1,2-dichloro-ethane

2: 5 percent / TMSOTf, Molekularsieb 4 Angstroem / CH₂Cl₂ / -50 °C

With 1H-imidazole; trimethylsilyl trifluoromethanesulfonate; Molekularsieb 4 Angstroem; In dichloromethane; 1,2-dichloro-ethane;