9-(3-methoxyphenyl)-3,3,6,6-tetramethyl-3,4,6,7,9,10-hexahydro-1,8(2H,5H)-acridinedione

Base Information

Chemical Name:9-(3-methoxyphenyl)-3,3,6,6-tetramethyl-3,4,6,7,9,10-hexahydro-1,8(2H,5H)-acridinedione
CAS No.:333353-84-7
Molecular Formula:C₂₄H₂₉NO₃
Molecular Weight:379.499
Hs Code.:

Synonyms:9-(3-methoxyphenyl)-3,3,6,6-tetramethyl-3,4,6,7,9,10-hexahydro-1,8(2H,5H)-acridinedione

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Chemical Property of 9-(3-methoxyphenyl)-3,3,6,6-tetramethyl-3,4,6,7,9,10-hexahydro-1,8(2H,5H)-acridinedione

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Technology Process of 9-(3-methoxyphenyl)-3,3,6,6-tetramethyl-3,4,6,7,9,10-hexahydro-1,8(2H,5H)-acridinedione

There total 6 articles about 9-(3-methoxyphenyl)-3,3,6,6-tetramethyl-3,4,6,7,9,10-hexahydro-1,8(2H,5H)-acridinedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 126-81-8
dimedone

: 591-31-1
3-methoxy-benzaldehyde

: 333353-84-7
9-(3-methoxyphenyl)-3,3,6,6-tetramethyl-3,4,6,7,9,10-hexahydro-1,8(2H,5H)-acridinedione

Guidance literature:: With ammonium acetate; In ethanol; at 75 ℃; for 2h;
DOI:10.1039/d0ra07986c

Reference yield: 75.0%

: 873-95-0
1-amino-5,5-dimethylcyclohexen-3-one

: 126-81-8
dimedone

: 591-31-1
3-methoxy-benzaldehyde

: 333353-84-7
9-(3-methoxyphenyl)-3,3,6,6-tetramethyl-3,4,6,7,9,10-hexahydro-1,8(2H,5H)-acridinedione

Guidance literature:: 1-amino-5,5-dimethylcyclohexen-3-one; 3-methoxy-benzaldehyde; In ethanol; at 100 ℃; for 0.333333h;

dimedone; In ethanol; at 100 ℃; for 3.5h;
DOI:10.1007/s11164-021-04643-z

Reference yield:

: 126-81-8
dimedone

: 591-31-1
3-methoxy-benzaldehyde

: 333353-84-7
9-(3-methoxyphenyl)-3,3,6,6-tetramethyl-3,4,6,7,9,10-hexahydro-1,8(2H,5H)-acridinedione

: 40588-53-2
9-(3-methoxyphenyl)-3,3,6,6-tetramethyl-3,4,5,6,7,9-hexahydro-1H-xanthene-1,8(2H)-dione

Guidance literature:: With ammonium acetate; acetic acid; In neat (no solvent); at 80 ℃; for 4h; Solvent; Temperature; Reagent/catalyst;
DOI:10.1007/s11164-021-04643-z