diethyl (4-fluorophenyl)hydroxymethylphosphonate

Base Information

Chemical Name:diethyl (4-fluorophenyl)hydroxymethylphosphonate
CAS No.:21386-00-5
Molecular Formula:C₁₁H₁₆FO₄P
Molecular Weight:262.218
Hs Code.:

Synonyms:diethyl (4-fluorophenyl)hydroxymethylphosphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl (4-fluorophenyl)hydroxymethylphosphonate

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Technology Process of diethyl (4-fluorophenyl)hydroxymethylphosphonate

There total 10 articles about diethyl (4-fluorophenyl)hydroxymethylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 459-57-4
4-fluorobenzaldehyde

: 762-04-9
phosphonic acid diethyl ester

: 21386-00-5
diethyl (4-fluorophenyl)hydroxymethylphosphonate

Guidance literature:: With C₄₆H₇₆N₅Si₂Sm; In toluene; at 20 ℃; Solvent; Schlenk technique; Inert atmosphere;
DOI:10.1007/s11426-012-4789-1

Reference yield: 94.0%

Diethyl phosphonate: 762-04-9,123-22-8
Diethyl phosphonate

: 459-57-4
4-fluorobenzaldehyde

: 21386-00-5
diethyl (4-fluorophenyl)hydroxymethylphosphonate

Guidance literature:: Diethyl phosphonate; With [(Me₃Si)₂N]₃La(μ-Cl)Li(THF)₃; In toluene; for 0.166667h; Inert atmosphere;

4-fluorobenzaldehyde; In toluene; at 25 ℃; for 0.0833333h; Inert atmosphere;
DOI:10.1021/jo101743e