C₁₉H₁₈ClNSi

Base Information

Chemical Name:C₁₉H₁₈ClNSi
CAS No.:1430235-72-5
Molecular Formula:C₁₉H₁₈ClNSi
Molecular Weight:323.897
Hs Code.:

Synonyms:C₁₉H₁₈ClNSi

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Chemical Property of C₁₉H₁₈ClNSi

Chemical Property:

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Technology Process of C₁₉H₁₈ClNSi

There total 5 articles about C₁₉H₁₈ClNSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1430235-07-6
C₁₉H₁₇ClFNSi

: 1430235-72-5
C₁₉H₁₈ClNSi

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at 0 - 20 ℃; for 2h;
DOI:10.1021/ol400977r

Reference yield:

: 100-43-6,329041-72-7
4-vinylpyridine

: 1430235-72-5
C₁₉H₁₈ClNSi

Guidance literature:: Multi-step reaction with 4 steps

1: bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; triphenylphosphine / tetrahydrofuran / 1 h / 90 °C / Glovebox; Inert atmosphere; Schlenk technique

2: (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 1,10-Phenanthroline; norborn-2-ene / tetrahydrofuran / 12 h / 90 °C / Glovebox; Inert atmosphere; Schlenk technique

3: silver fluoride; N-chloro-succinimide / toluene / 2 h / 20 °C / Darkness

4: lithium aluminium tetrahydride / diethyl ether / 2 h / 0 - 20 °C

With norborn-2-ene; bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; N-chloro-succinimide; lithium aluminium tetrahydride; 1,10-Phenanthroline; (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; silver fluoride; triphenylphosphine; In tetrahydrofuran; diethyl ether; toluene;
DOI:10.1021/ol400977r

Reference yield:

: 1430235-05-4
C₁₉H₁₇NSi

: 1430235-72-5
C₁₉H₁₈ClNSi

Guidance literature:: Multi-step reaction with 2 steps

1: silver fluoride; N-chloro-succinimide / toluene / 2 h / 20 °C / Darkness

2: lithium aluminium tetrahydride / diethyl ether / 2 h / 0 - 20 °C

With N-chloro-succinimide; lithium aluminium tetrahydride; silver fluoride; In diethyl ether; toluene;
DOI:10.1021/ol400977r