1-hydroxy-2-phenyl-2-(4-tert-butoxycarbonylamino-2,2,6,6-tetramethyl-1-piperidinyloxy)ethane

Base Information

Chemical Name:1-hydroxy-2-phenyl-2-(4-tert-butoxycarbonylamino-2,2,6,6-tetramethyl-1-piperidinyloxy)ethane
CAS No.:213994-50-4
Molecular Formula:C₂₂H₃₆N₂O₄
Molecular Weight:392.539
Hs Code.:

Synonyms:1-hydroxy-2-phenyl-2-(4-tert-butoxycarbonylamino-2,2,6,6-tetramethyl-1-piperidinyloxy)ethane

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Chemical Property of 1-hydroxy-2-phenyl-2-(4-tert-butoxycarbonylamino-2,2,6,6-tetramethyl-1-piperidinyloxy)ethane

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Technology Process of 1-hydroxy-2-phenyl-2-(4-tert-butoxycarbonylamino-2,2,6,6-tetramethyl-1-piperidinyloxy)ethane

There total 4 articles about 1-hydroxy-2-phenyl-2-(4-tert-butoxycarbonylamino-2,2,6,6-tetramethyl-1-piperidinyloxy)ethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 423126-07-2
1-benzoyloxy-(4-tert-butoxycarbonylamino)-2-phenyl-2-(2,2,6,6-tetramethyl-1-piperidinyloxy)ethane

: 213994-50-4
1-hydroxy-2-phenyl-2-(4-tert-butoxycarbonylamino-2,2,6,6-tetramethyl-1-piperidinyloxy)ethane

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; methanol; for 8h; Ambient temperature;
DOI:10.1021/ja980241v

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 213994-50-4
1-hydroxy-2-phenyl-2-(4-tert-butoxycarbonylamino-2,2,6,6-tetramethyl-1-piperidinyloxy)ethane

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / diisopropylethylamine / CH₂Cl₂ / 4 h / Ambient temperature

2: 38 percent / 50 °C

3: 98 percent / 10 N aq. NaOH / tetrahydrofuran; methanol / 8 h / Ambient temperature

With sodium hydroxide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/ja980241v

Reference yield:

: 14691-88-4,78774-22-8
4-amino-2,2,6,6-tetramethyl-1-piperidine-1-oxyl

: 213994-50-4
1-hydroxy-2-phenyl-2-(4-tert-butoxycarbonylamino-2,2,6,6-tetramethyl-1-piperidinyloxy)ethane

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / diisopropylethylamine / CH₂Cl₂ / 4 h / Ambient temperature

2: 38 percent / 50 °C

3: 98 percent / 10 N aq. NaOH / tetrahydrofuran; methanol / 8 h / Ambient temperature

With sodium hydroxide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/ja980241v