C₃₉H₄₂FN₅O₅

Base Information

Chemical Name:C₃₉H₄₂FN₅O₅
CAS No.:639492-24-3
Molecular Formula:C₃₉H₄₂FN₅O₅
Molecular Weight:679.791
Hs Code.:

C<sub>39</sub>H<sub>42</sub>FN<sub>5</sub>O<sub>5</sub>

Synonyms:C₃₉H₄₂FN₅O₅

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Chemical Property of C₃₉H₄₂FN₅O₅

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Technology Process of C₃₉H₄₂FN₅O₅

There total 7 articles about C₃₉H₄₂FN₅O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 639492-08-3
C₃₉H₄₄FN₅O₆

: 639492-24-3
C₃₉H₄₂FN₅O₅

Guidance literature:: With (bis-(2-methoxyethyl)amino)sulfur trufluoride; In dichloromethane; at -20 ℃; for 3h;
DOI:10.1016/j.tet.2003.04.008

Reference yield:

: 100-83-4
meta-hydroxybenzaldehyde

: 639492-24-3
C₃₉H₄₂FN₅O₅

Guidance literature:: Multi-step reaction with 9 steps

1: 60 percent / Cs₂CO₃ / dimethylformamide / 115 °C

2: tetrahydrofuran / 0.75 h / -70 - 20 °C

3: 46.0 g / p-dimethylaminopyridine / CH₂Cl₂ / 3.5 h / 20 °C

4: 77 percent / HF; pyridine / 4 h / 20 °C

5: 74 percent / Dess-Martin periodinane; pyridine / CH₂Cl₂ / 3 h / 4 - 20 °C

6: K₂CO₃ / dimethylformamide / 5 h / 20 °C

7: dimethylformamide / 17 h / 20 °C

8: 61 percent / C39H32OP2 bis-phosphine; [(η³-allyl)PdCl]2 / tetrahydrofuran; dimethylformamide / 1 h / 20 °C

9: 57 percent / bis(2-methoxyethyl)aminosulfur trifluoride / CH₂Cl₂ / 3 h / -20 °C

With pyridine; dmap; bis(η3-allyl-μ-chloropalladium(II)); C₃₉H₃₂OP₂ bis-phosphine; hydrogen fluoride; potassium carbonate; caesium carbonate; Dess-Martin periodane; (bis-(2-methoxyethyl)amino)sulfur trufluoride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2003.04.008

Reference yield:

: 692729-77-4
3-[4-(tert-butyl-dimethyl-silanyloxy)-butoxy]-benzaldehyde

: 639492-24-3
C₃₉H₄₂FN₅O₅

Guidance literature:: Multi-step reaction with 8 steps

1: tetrahydrofuran / 0.75 h / -70 - 20 °C

2: 46.0 g / p-dimethylaminopyridine / CH₂Cl₂ / 3.5 h / 20 °C

3: 77 percent / HF; pyridine / 4 h / 20 °C

4: 74 percent / Dess-Martin periodinane; pyridine / CH₂Cl₂ / 3 h / 4 - 20 °C

5: K₂CO₃ / dimethylformamide / 5 h / 20 °C

6: dimethylformamide / 17 h / 20 °C

7: 61 percent / C39H32OP2 bis-phosphine; [(η³-allyl)PdCl]2 / tetrahydrofuran; dimethylformamide / 1 h / 20 °C

8: 57 percent / bis(2-methoxyethyl)aminosulfur trifluoride / CH₂Cl₂ / 3 h / -20 °C

With pyridine; dmap; bis(η3-allyl-μ-chloropalladium(II)); C₃₉H₃₂OP₂ bis-phosphine; hydrogen fluoride; potassium carbonate; Dess-Martin periodane; (bis-(2-methoxyethyl)amino)sulfur trufluoride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2003.04.008