4-[1-oxo-3-(3,4,5-trimethoxyphenyl)-2-propenyl]-3-(3-chloro-4-fluorophenyl)sydnone

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Chemical Name:4-[1-oxo-3-(3,4,5-trimethoxyphenyl)-2-propenyl]-3-(3-chloro-4-fluorophenyl)sydnone
CAS No.:1366133-64-3
Molecular Formula:C₂₀H₁₆ClFN₂O₆
Molecular Weight:434.808
Hs Code.:

Synonyms:4-[1-oxo-3-(3,4,5-trimethoxyphenyl)-2-propenyl]-3-(3-chloro-4-fluorophenyl)sydnone

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Chemical Property of 4-[1-oxo-3-(3,4,5-trimethoxyphenyl)-2-propenyl]-3-(3-chloro-4-fluorophenyl)sydnone

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Technology Process of 4-[1-oxo-3-(3,4,5-trimethoxyphenyl)-2-propenyl]-3-(3-chloro-4-fluorophenyl)sydnone

There total 2 articles about 4-[1-oxo-3-(3,4,5-trimethoxyphenyl)-2-propenyl]-3-(3-chloro-4-fluorophenyl)sydnone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1366133-70-1
4-acetyl-3-(3-chloro-4-fluorophenyl)sydnone

: 86-81-7
3,4,5-trimethoxy-benzaldehyde

: 1366133-64-3
4-[1-oxo-3-(3,4,5-trimethoxyphenyl)-2-propenyl]-3-(3-chloro-4-fluorophenyl)sydnone

Guidance literature:: With sodium hydroxide; In ethanol; water; at 5 - 10 ℃; for 0.333333h; Sonication;
DOI:10.14233/ajchem.2015.18864

Reference yield:

: 68657-50-1
3-(3-chloro-4-fluorophenyl)sydnone

: 1366133-64-3
4-[1-oxo-3-(3,4,5-trimethoxyphenyl)-2-propenyl]-3-(3-chloro-4-fluorophenyl)sydnone

Guidance literature:: Multi-step reaction with 2 steps

1: phosphorus pentoxide

2: sodium hydroxide / ethanol; water / 1 h / 5 - 10 °C

With phosphorus pentoxide; sodium hydroxide; In ethanol; water; 2: Claisen-Schmidt reaction;
DOI:10.3109/14756366.2011.586345