N-(1-benzothiophen-2-yl(2-(methylsulfanyl)phenyl)methyl)-2-methyl-2-propanesulfinamide

Base Information

• Chemical Name: N-(1-benzothiophen-2-yl(2-(methylsulfanyl)phenyl)methyl)-2-methyl-2-propanesulfinamide
• CAS No.: 1402599-53-4
• Molecular Formula: C₂₀H₂₃NOS₃
• Molecular Weight: 389.607

Synonyms:N-(1-benzothiophen-2-yl(2-(methylsulfanyl)phenyl)methyl)-2-methyl-2-propanesulfinamide

Chemical Property of N-(1-benzothiophen-2-yl(2-(methylsulfanyl)phenyl)methyl)-2-methyl-2-propanesulfinamide

Chemical Property:

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Technology Process of N-(1-benzothiophen-2-yl(2-(methylsulfanyl)phenyl)methyl)-2-methyl-2-propanesulfinamide

There total 2 articles about N-(1-benzothiophen-2-yl(2-(methylsulfanyl)phenyl)methyl)-2-methyl-2-propanesulfinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(1-benzothiophen-2-ylmethylidene)-2-methyl-2-propanesulfinamide (1402599-52-3) + [2-(methylsulfanyl)phenyl]magnesium bromide (99346-84-6) → N-(1-benzothiophen-2-yl(2-(methylsulfanyl)phenyl)methyl)-2-methyl-2-propanesulfinamide (1402599-53-4)

Guidance literature:

N-(1-benzothiophen-2-ylmethylidene)-2-methyl-2-propanesulfinamide; (2-(methylthio)phenyl)magnesium bromide; In tetrahydrofuran; at 20 ℃; for 96h;

With water; sodium hydrogencarbonate; In tetrahydrofuran;

Reference yield:

benzothiophene-2-carboxaldehyde (3541-37-5) → N-(1-benzothiophen-2-yl(2-(methylsulfanyl)phenyl)methyl)-2-methyl-2-propanesulfinamide (1402599-53-4)

Guidance literature:

Multi-step reaction with 2 steps

1: copper(II) sulfate / dichloromethane / 15 h / 20 °C

2: tetrahydrofuran / 96 h / 20 °C

With copper(II) sulfate; In tetrahydrofuran; dichloromethane;

Reference yield:

N-(1-benzothiophen-2-yl(2-(methylsulfanyl)phenyl)methyl)-2-methyl-2-propanesulfinamide (1402599-53-4) → 1-(1-benzothiophen-2-yl)-1-(2-(methylsulfanyl)phenyl)methanamine (1402599-51-2)

Guidance literature:

N-(1-benzothiophen-2-yl(2-(methylsulfanyl)phenyl)methyl)-2-methyl-2-propanesulfinamide; With hydrogenchloride; In diethyl ether; at 20 ℃; for 3h;

With sodium hydrogencarbonate; In water; ethyl acetate;

upstream raw materials:

benzothiophene-2-carboxaldehyde

N-(1-benzothiophen-2-ylmethylidene)-2-methyl-2-propanesulfinamide

[2-(methylsulfanyl)phenyl]magnesium bromide

Downstream raw materials:

1-(1-benzothiophen-2-yl)-1-(2-(methylsulfanyl)phenyl)methanamine

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