C₁₅H₂₀O

Base Information

Chemical Name:C₁₅H₂₀O
CAS No.:1004539-90-5
Molecular Formula:C₁₅H₂₀O
Molecular Weight:216.323
Hs Code.:

Synonyms:C₁₅H₂₀O

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Chemical Property of C₁₅H₂₀O

Chemical Property:

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Technology Process of C₁₅H₂₀O

There total 7 articles about C₁₅H₂₀O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: C₂₇H₄₀N₂O₄SSi

: 1004539-90-5
C₁₅H₂₀O

Guidance literature:: C₂₇H₄₀N₂O₄SSi; With silica gel; benzo[1,3,2]dioxaborole; In chloroform; at -42 ℃; for 1h;

With sodium acetate; In chloroform; for 16h; Further stages.; Heating;
DOI:10.1021/ol702921x

Reference yield: 81.0%

: C₂₂H₂₆N₂O₃S

: 1004539-90-5
C₁₅H₂₀O

Guidance literature:: C₂₂H₂₆N₂O₃S; With silica gel; benzo[1,3,2]dioxaborole; In chloroform; at -42 - 20 ℃; for 1h; Inert atmosphere;

With sodium acetate; In chloroform; for 16h; Inert atmosphere; Reflux;
DOI:10.1021/acs.joc.7b00428

Reference yield:

: 33106-32-0
(S)-2-(benzyloxy)propanoic acid

: 1004539-90-5
C₁₅H₂₀O

Guidance literature:: Multi-step reaction with 4 steps

1.1: pivaloyl chloride; triethylamine / 0.5 h / 0 °C / Inert atmosphere

1.2: 16 h / 20 °C / Inert atmosphere

2.1: n-butyllithium / diethyl ether; hexane / 0.5 h / -78 °C / Inert atmosphere

2.2: 0.01 h / -78 °C / Inert atmosphere

3.1: titanium(IV) isopropylate / 16 h / 20 °C / Inert atmosphere

4.1: benzo[1,3,2]dioxaborole; silica gel / chloroform / 1 h / -42 - 20 °C / Inert atmosphere

4.2: 16 h / Inert atmosphere; Reflux

With titanium(IV) isopropylate; n-butyllithium; pivaloyl chloride; silica gel; triethylamine; benzo[1,3,2]dioxaborole; In diethyl ether; hexane; chloroform;
DOI:10.1021/acs.joc.7b00428