benzoic acid (Z)-2-hydroxyiminoethyl ester

Base Information

Chemical Name:benzoic acid (Z)-2-hydroxyiminoethyl ester
CAS No.:1285526-84-2
Molecular Formula:C₉H₉NO₃
Molecular Weight:179.175
Hs Code.:

Synonyms:benzoic acid (Z)-2-hydroxyiminoethyl ester

Suppliers and Price of benzoic acid (Z)-2-hydroxyiminoethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of benzoic acid (Z)-2-hydroxyiminoethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of benzoic acid (Z)-2-hydroxyiminoethyl ester

There total 3 articles about benzoic acid (Z)-2-hydroxyiminoethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 1285526-77-3
C₁₈H₁₈N₂O₆

: 1285526-84-2
benzoic acid (Z)-2-hydroxyiminoethyl ester

: benzoic acid (E)-2-hydroxyiminoethyl ester

Guidance literature:: In toluene; optical yield given as %de; Inert atmosphere; Reflux;
DOI:10.1016/j.tet.2011.01.054

Reference yield:

: 7127-19-7
2-phenyl-1,3-oxazoline

: 1285526-84-2
benzoic acid (Z)-2-hydroxyiminoethyl ester

: benzoic acid (E)-2-hydroxyiminoethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 12 h / 20 °C / Cooling with ice

2: toluene / Inert atmosphere; Reflux

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; toluene;
DOI:10.1016/j.tet.2011.01.054

Reference yield:

: 102588-18-1
O-(trimethylsilyl)-N-((trimethylsilyl)oxy)-N-vinylhydroxylamine

: 65-85-0,8013-63-6
benzoic acid

: 1285526-84-2
benzoic acid (Z)-2-hydroxyiminoethyl ester

: benzoic acid (E)-2-hydroxyiminoethyl ester

Guidance literature:: In dichloromethane; N,N-dimethyl-formamide; at 20 ℃; for 2h; Overall yield = 99 %; Overall yield = 353 mg; regioselective reaction;
DOI:10.1002/ejoc.201701266