S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-ethyl sulfoximide

Base Information

Chemical Name:S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-ethyl sulfoximide
CAS No.:1147095-61-1
Molecular Formula:C₂₁H₁₈Cl₂N₄O₃S
Molecular Weight:477.371
Hs Code.:

Synonyms:S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-ethyl sulfoximide

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Chemical Property of S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-ethyl sulfoximide

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Technology Process of S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-ethyl sulfoximide

There total 10 articles about S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-ethyl sulfoximide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1147095-61-1
S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-ethyl sulfoximide

Guidance literature:

Reference yield:

: C₂₉H₂₄Cl₂N₄O₅S

: 1147095-61-1
S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-ethyl sulfoximide

Guidance literature:: With sulfuric acid; at 0 - 5 ℃;
DOI:10.1016/j.ejmech.2012.10.005

Reference yield:

: 99186-27-3
methyl 4-(ethylthio)benzoate

: 1147095-61-1
S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-ethyl sulfoximide

Guidance literature:: Multi-step reaction with 7 steps

1: dihydrogen peroxide; vanadium(V) oxide / acetonitrile / 5 h / -20 - 30 °C / Inert atmosphere

2: sodium azide; sulfuric acid / chloroform / 15 h / -20 - 50 °C / Inert atmosphere

3: pyridine / dichloromethane; toluene / 3 h / 15 - 30 °C / Inert atmosphere

4: water; sodium hydroxide / tetrahydrofuran / 3 h / 25 - 30 °C

5: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 3 h / 10 - 30 °C / Inert atmosphere

6: tetrahydrofuran / 2 h / 10 - 30 °C / Inert atmosphere

7: sulfuric acid / 0 - 5 °C

With pyridine; sodium azide; vanadium(V) oxide; oxalyl dichloride; sulfuric acid; water; dihydrogen peroxide; N,N-dimethyl-formamide; sodium hydroxide; In tetrahydrofuran; dichloromethane; chloroform; toluene; acetonitrile;
DOI:10.1016/j.ejmech.2012.10.005