C₄₆H₇₆O₇Si₂

Base Information

Chemical Name:C₄₆H₇₆O₇Si₂
CAS No.:1122481-15-5
Molecular Formula:C₄₆H₇₆O₇Si₂
Molecular Weight:797.276
Hs Code.:

C<sub>46</sub>H<sub>76</sub>O<sub>7</sub>Si<sub>2</sub>

Synonyms:C₄₆H₇₆O₇Si₂

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Chemical Property of C₄₆H₇₆O₇Si₂

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Technology Process of C₄₆H₇₆O₇Si₂

There total 14 articles about C₄₆H₇₆O₇Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 944393-23-1
C₃₁H₅₄O₅Si₂

: 1122481-11-1
C₁₈H₃₀O₂Si

: 1122481-15-5
C₄₆H₇₆O₇Si₂

Guidance literature:: C₃₁H₅₄O₅Si₂; C₁₈H₃₀O₂Si; With boron trifluoride diethyl etherate; In dichloromethane; at -78 ℃; Inert atmosphere;

With water; sodium hydrogencarbonate; In dichloromethane; optical yield given as %de; Inert atmosphere;
DOI:10.1021/ol802772s

Reference yield:

: C₃₁H₅₈O₆Si₂

: 1122481-15-5
C₄₆H₇₆O₇Si₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium periodate / methanol; water / 1 h / 20 °C

2.1: n-butyllithium; potassium tert-butylate / tetrahydrofuran; hexane / 0.67 h / -78 - -46 °C

2.2: -78 °C

3.1: amberlyst resin / dichloromethane / 2 h / 20 °C

4.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water; tert-butyl alcohol / 0 - 20 °C

4.2: 5 h

5.1: sodium periodate / methanol; water / 1 h / 20 °C

6.1: boron trifluoride diethyl etherate / dichloromethane / -78 °C

With sodium periodate; osmium(VIII) oxide; n-butyllithium; boron trifluoride diethyl etherate; potassium tert-butylate; 4-methylmorpholine N-oxide; amberlyst resin; In tetrahydrofuran; methanol; hexane; dichloromethane; water; tert-butyl alcohol;

Reference yield:

: 944393-25-3
C₃₄H₆₂O₅Si₂

: 1122481-15-5
C₄₆H₇₆O₇Si₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: amberlyst resin / dichloromethane / 2 h / 20 °C

2.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water; tert-butyl alcohol / 0 - 20 °C

2.2: 5 h

3.1: sodium periodate / methanol; water / 1 h / 20 °C

4.1: boron trifluoride diethyl etherate / dichloromethane / -78 °C

With sodium periodate; osmium(VIII) oxide; boron trifluoride diethyl etherate; 4-methylmorpholine N-oxide; amberlyst resin; In tetrahydrofuran; methanol; dichloromethane; water; tert-butyl alcohol;