2,6-dimethylphenyl 3-O-benzoyl-6-O-benzyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:2,6-dimethylphenyl 3-O-benzoyl-6-O-benzyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-1-thio-β-D-glucopyranoside
CAS No.:1163124-28-4
Molecular Formula:C₃₁H₃₂Cl₃NO₇S
Molecular Weight:669.023
Hs Code.:

Synonyms:2,6-dimethylphenyl 3-O-benzoyl-6-O-benzyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-1-thio-β-D-glucopyranoside

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Chemical Property of 2,6-dimethylphenyl 3-O-benzoyl-6-O-benzyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-1-thio-β-D-glucopyranoside

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Technology Process of 2,6-dimethylphenyl 3-O-benzoyl-6-O-benzyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-1-thio-β-D-glucopyranoside

There total 1 articles about 2,6-dimethylphenyl 3-O-benzoyl-6-O-benzyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1163124-27-3
2,6-dimethylphenyl 3-O-benzoyl-4,6-O-benzylidene-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-1-thio-β-D-glucopyranoside

: 1163124-28-4
2,6-dimethylphenyl 3-O-benzoyl-6-O-benzyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-1-thio-β-D-glucopyranoside

Guidance literature:: With hydrogenchloride; sodium cyanoborohydride; In tetrahydrofuran; diethyl ether; at 0 ℃; for 0.5h;
DOI:10.1016/j.carres.2009.02.019

Reference yield: 86.0%

: 1163124-28-4
2,6-dimethylphenyl 3-O-benzoyl-6-O-benzyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-1-thio-β-D-glucopyranoside

: 74808-10-9,86520-63-0,87119-53-7,92052-29-4,121238-27-5,142831-80-9,127061-80-7
2,3,4,6-tetra-O-acetyl-D-galactopyranosyl trichloroacetimidate

: 1163124-29-5
2,6-dimethylphenyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1->4)-3-O-benzoyl-6-O-benzyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-1-thio-β-D-glucopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -20 ℃; for 1h;
DOI:10.1016/j.carres.2009.02.019

Reference yield: 78.0%

: 2-O-benzoyl-3,6-di-O-benzyl-4-O-chloroacetyl-D-galactopyranosyl fluoride

: 1163124-28-4
2,6-dimethylphenyl 3-O-benzoyl-6-O-benzyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-1-thio-β-D-glucopyranoside

: 1163124-35-3
2,6-dimethylphenyl 2-O-benzoyl-3,6-di-O-benzyl-4-O-chloroacetyl-β-D-galactopyranosyl-(1->4)-3-O-benzoyl-6-O-benzyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-1-thio-β-D-glucopyranoside

Guidance literature:: With Cp₂HfCl₂; silver trifluoromethanesulfonate; In dichloromethane; at -20 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.carres.2009.02.019