9,9-dioctadecanyl-2-diphenylaminofluorene

Base Information

• Chemical Name: 9,9-dioctadecanyl-2-diphenylaminofluorene
• CAS No.: 1449395-05-4
• Molecular Formula: C₆₁H₉₁N
• Molecular Weight: 838.4
• Mol file: 1449395-05-4.mol

Synonyms:9,9-dioctadecanyl-2-diphenylaminofluorene

Chemical Property of 9,9-dioctadecanyl-2-diphenylaminofluorene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 9,9-dioctadecanyl-2-diphenylaminofluorene

There total 2 articles about 9,9-dioctadecanyl-2-diphenylaminofluorene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

C25H19N (870133-75-8) + 1-Bromooctadecane (112-89-0) → 9,9-dioctadecanyl-2-diphenylaminofluorene (1449395-05-4)

Guidance literature:

With potassium tert-butylate; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

DOI:10.3390/molecules18089603

Reference yield:

2-bromo-9H-fluorene (1133-80-8) → 9,9-dioctadecanyl-2-diphenylaminofluorene (1449395-05-4)

Guidance literature:

Multi-step reaction with 2 steps

1: Palladium catalyst

2: potassium tert-butylate / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

With potassium tert-butylate; In tetrahydrofuran;

DOI:10.3390/molecules18089603

Reference yield: 96.0%

9,9-dioctadecanyl-2-diphenylaminofluorene (1449395-05-4) + 2-Bromoacetyl bromide (598-21-0) → 7-α-bromoacetyl-9,9-dioctadecanyl-2-diphenylaminofluorene (868852-16-8)

Guidance literature:

With aluminum (III) chloride; In 1,2-dichloro-ethane; at 0 ℃; for 4h;

DOI:10.3390/molecules18089603

upstream raw materials:

C₂₅H₁₉N

1-Bromooctadecane

2-bromo-9H-fluorene

Downstream raw materials:

7-α-bromoacetyl-9,9-dioctadecanyl-2-diphenylaminofluorene