L-[1,2,3-¹³C₃,¹⁵N]alanyl-D-α-glutamine phenylmethyl ester hydrochloride

Base Information

Chemical Name:L-[1,2,3-¹³C₃,¹⁵N]alanyl-D-α-glutamine phenylmethyl ester hydrochloride
CAS No.:1467710-19-5
Molecular Formula:C₁₅H₂₁N₃O₄*ClH
Molecular Weight:347.771
Hs Code.:

L-[1,2,3-<sup>13</sup>C<sub>3</sub>,<sup> 15</sup>N]alanyl-D-α-glutamine phenylmethyl ester hydrochloride

Synonyms:L-[1,2,3-¹³C₃,¹⁵N]alanyl-D-α-glutamine phenylmethyl ester hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of L-[1,2,3-¹³C₃,¹⁵N]alanyl-D-α-glutamine phenylmethyl ester hydrochloride

Chemical Property:

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Technology Process of L-[1,2,3-¹³C₃,¹⁵N]alanyl-D-α-glutamine phenylmethyl ester hydrochloride

There total 2 articles about L-[1,2,3-¹³C₃,¹⁵N]alanyl-D-α-glutamine phenylmethyl ester hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1467710-17-3
N-[(1,1-dimethylethoxy)carbonyl]-L-[1,2,3-¹³C₃,¹⁵N]alanyl-D-α-glutamine phenylmethyl ester

: 1467710-19-5
L-[1,2,3-¹³C₃,¹⁵N]alanyl-D-α-glutamine phenylmethyl ester hydrochloride

Guidance literature:: With hydrogenchloride; In di-isopropyl ether; at 20 ℃;
DOI:10.1002/jlcr.3078

Reference yield:

: 71811-14-8,80064-48-8
D-Glutaminsaeure-α-amid-γ-benzylester

: 1467710-19-5
L-[1,2,3-¹³C₃,¹⁵N]alanyl-D-α-glutamine phenylmethyl ester hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: 4-methyl-morpholine / N,N-dimethyl-formamide; ethyl acetate / -10 °C

1.3: 0.5 h / -5 °C

2.1: hydrogenchloride / di-isopropyl ether / 20 °C

With 4-methyl-morpholine; hydrogenchloride; In di-isopropyl ether; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1002/jlcr.3078

Reference yield: 98.0%

: 1467710-19-5
L-[1,2,3-¹³C₃,¹⁵N]alanyl-D-α-glutamine phenylmethyl ester hydrochloride

: 1467710-22-0
C₂₁H₂₉NO₈

: 1467710-25-3
N²-[N-(N-acetyl)-4,6-O-(1-methylethylidene)-1-O-(phenylmethyl)-α-muramoyl]-L-[1,2,3-¹³C₃,¹⁵N]alanyl-D-α-glutamine phenylmethyl ester

Guidance literature:: L-[1,2,3-¹³C₃,¹⁵N]alanyl-D-α-glutamine phenylmethyl ester hydrochloride; C₂₁H₂₉NO₈; With 1-hydroxy-pyrrolidine-2,5-dione; triethylamine; In ethyl acetate;

With dicyclohexyl-carbodiimide; at 20 ℃; for 2.5h;
DOI:10.1002/jlcr.3078