5,5'-((pyridine-3,5-dicarbonyl)bis(azanediyl))diisophthalic acid

Base Information

Chemical Name:5,5'-((pyridine-3,5-dicarbonyl)bis(azanediyl))diisophthalic acid
CAS No.:1402171-58-7
Molecular Formula:C₂₃H₁₅N₃O₁₀
Molecular Weight:493.386
Hs Code.:

Synonyms:5,5'-((pyridine-3,5-dicarbonyl)bis(azanediyl))diisophthalic acid

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Chemical Property of 5,5'-((pyridine-3,5-dicarbonyl)bis(azanediyl))diisophthalic acid

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Technology Process of 5,5'-((pyridine-3,5-dicarbonyl)bis(azanediyl))diisophthalic acid

There total 2 articles about 5,5'-((pyridine-3,5-dicarbonyl)bis(azanediyl))diisophthalic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15074-61-0
pyridine-3,5-dicarbonyl dichloride

: 99-31-0
5-aminoisophthalic acid

: 1402171-58-7
5,5'-((pyridine-3,5-dicarbonyl)bis(azanediyl))diisophthalic acid

Guidance literature:: In acetonitrile; at 20 ℃; Reflux;
DOI:10.1039/c2cc34622b

Reference yield:

: 499-81-0
3,5-Pyridinedicarboxylic acid

: 1402171-58-7
5,5'-((pyridine-3,5-dicarbonyl)bis(azanediyl))diisophthalic acid

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / Inert atmosphere; Reflux

2: dmap / N,N-dimethyl acetamide / 49 h / 0 - 20 °C / Inert atmosphere

With dmap; thionyl chloride; In N,N-dimethyl acetamide;
DOI:10.1002/chem.201504907