4-[3-(1-ethoxycarbonylpiperidine-4-yl)-4,4-dimethyl-5-oxo-2-thioxoimidazolidin-1-yl]-2-trifluoromethylbenzonitrile

Base Information

Chemical Name:4-[3-(1-ethoxycarbonylpiperidine-4-yl)-4,4-dimethyl-5-oxo-2-thioxoimidazolidin-1-yl]-2-trifluoromethylbenzonitrile
CAS No.:879613-07-7
Molecular Formula:C₂₁H₂₃F₃N₄O₃S
Molecular Weight:468.5
Hs Code.:

Synonyms:4-[3-(1-ethoxycarbonylpiperidine-4-yl)-4,4-dimethyl-5-oxo-2-thioxoimidazolidin-1-yl]-2-trifluoromethylbenzonitrile

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Chemical Property of 4-[3-(1-ethoxycarbonylpiperidine-4-yl)-4,4-dimethyl-5-oxo-2-thioxoimidazolidin-1-yl]-2-trifluoromethylbenzonitrile

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Technology Process of 4-[3-(1-ethoxycarbonylpiperidine-4-yl)-4,4-dimethyl-5-oxo-2-thioxoimidazolidin-1-yl]-2-trifluoromethylbenzonitrile

There total 1 articles about 4-[3-(1-ethoxycarbonylpiperidine-4-yl)-4,4-dimethyl-5-oxo-2-thioxoimidazolidin-1-yl]-2-trifluoromethylbenzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: C₁₃H₂₄N₂O₄

: 143782-23-4
4-isothiocyanato 2-(trifluoromethyl)benzonitrile

: 879613-07-7
4-[3-(1-ethoxycarbonylpiperidine-4-yl)-4,4-dimethyl-5-oxo-2-thioxoimidazolidin-1-yl]-2-trifluoromethylbenzonitrile

Guidance literature:: With dimethylaminopyridine; In 1,2-dichloro-ethane; at 100 ℃; for 1h;

Reference yield: 91.0%

: 879613-07-7
4-[3-(1-ethoxycarbonylpiperidine-4-yl)-4,4-dimethyl-5-oxo-2-thioxoimidazolidin-1-yl]-2-trifluoromethylbenzonitrile

: C₁₈H₁₉F₃N₄OS*ClH

Guidance literature:: 4-[3-(1-ethoxycarbonylpiperidine-4-yl)-4,4-dimethyl-5-oxo-2-thioxoimidazolidin-1-yl]-2-trifluoromethylbenzonitrile; With hydrogenchloride; In 1,4-dioxane; at 100 ℃;

With sodium hydroxide; In 1,4-dioxane; water; pH=~ 10;

With hydrogenchloride; In 1,4-dioxane; ethyl acetate; at 0 ℃;

Reference yield: 75.0%

: 879613-07-7
4-[3-(1-ethoxycarbonylpiperidine-4-yl)-4,4-dimethyl-5-oxo-2-thioxoimidazolidin-1-yl]-2-trifluoromethylbenzonitrile

: 879614-70-7
4-(4,4-dimethyl-5-oxo-3-(piperidin-4-yl)-2-thioxoimidazolidin-1-yl)-2-(trifluoromethyl)benzonitrile

Guidance literature:: 4-[3-(1-ethoxycarbonylpiperidine-4-yl)-4,4-dimethyl-5-oxo-2-thioxoimidazolidin-1-yl]-2-trifluoromethylbenzonitrile; With hydrogenchloride; In 1,4-dioxane; water; Heating / reflux;

With sodium hydroxide; In 1,4-dioxane; water; pH=~ 10;