C₁₄H₂₆O₂

Base Information

• Chemical Name: C₁₄H₂₆O₂
• CAS No.: 1383153-62-5
• Molecular Formula: C₁₄H₂₆O₂
• Molecular Weight: 226.359
• Mol file: 1383153-62-5.mol

Synonyms:C₁₄H₂₆O₂

Chemical Property of C₁₄H₂₆O₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₄H₂₆O₂

There total 5 articles about C₁₄H₂₆O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C14H28O2 (1383149-67-4) → C14H26O2 (1383153-62-5)

Guidance literature:

With silica gel; pyridinium chlorochromate; In dichloromethane; at 20 ℃; for 4h; Inert atmosphere;

DOI:10.1021/jm300171v

Reference yield:

1,6-hexanediol (629-11-8) → C14H26O2 (1383153-62-5)

Guidance literature:

Multi-step reaction with 5 steps

1.1: 18-crown-6 ether; potassium hydroxide / tetrahydrofuran / 48 h / 0 - 20 °C

2.1: pyridine / 3 h / 0 °C

3.1: sodium hydride / N,N-dimethyl-formamide / 1.5 h / 20 °C

3.2: 1 h / 75 °C

4.1: palladium 10% on activated carbon; hydrogen / ethanol / 24 h

5.1: silica gel; pyridinium chlorochromate / dichloromethane / 4 h / 20 °C / Inert atmosphere

With pyridine; 18-crown-6 ether; palladium 10% on activated carbon; hydrogen; silica gel; sodium hydride; pyridinium chlorochromate; potassium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1021/jm300171v

Reference yield:

6-(benzyloxy)hexan-1-ol methanesulfonate (170656-31-2) → C14H26O2 (1383153-62-5)

Guidance literature:

Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 1.5 h / 20 °C

1.2: 1 h / 75 °C

2.1: palladium 10% on activated carbon; hydrogen / ethanol / 24 h

3.1: silica gel; pyridinium chlorochromate / dichloromethane / 4 h / 20 °C / Inert atmosphere

With palladium 10% on activated carbon; hydrogen; silica gel; sodium hydride; pyridinium chlorochromate; In ethanol; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1021/jm300171v

upstream raw materials:

C₂₁H₃₄O₂

C₁₄H₂₈O₂

1,6-hexanediol

1-bromo-6-hexanol

Downstream raw materials:

(2R,3R,4R,5S)-1-(6-((2,3-dimethylcyclohexyl)oxy)hexyl)-2-(hydroxymethyl)piperidine-3,4,5-triol