C₄₈H₆₈O₉Si

Base Information

Chemical Name:C₄₈H₆₈O₉Si
CAS No.:1449419-31-1
Molecular Formula:C₄₈H₆₈O₉Si
Molecular Weight:817.148
Hs Code.:

C<sub>48</sub>H<sub>68</sub>O<sub>9</sub>Si

Synonyms:C₄₈H₆₈O₉Si

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Chemical Property of C₄₈H₆₈O₉Si

Chemical Property:

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Technology Process of C₄₈H₆₈O₉Si

There total 9 articles about C₄₈H₆₈O₉Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1449419-37-7
C₄₉H₇₀O₇Si

: 1449419-31-1
C₄₈H₆₈O₉Si

Guidance literature:: With potassium permanganate; sodium periodate; In aq. phosphate buffer; tert-butyl alcohol; at 20 ℃; for 0.133333h; pH=7.2; Inert atmosphere;
DOI:10.1016/j.tet.2013.02.008

Reference yield:

: 1449419-34-4
C₄₃H₅₆O₇

: 1449419-31-1
C₄₈H₆₈O₉Si

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-imidazole / tetrahydrofuran / 4 h / 20 °C

2: sodium periodate; potassium permanganate / tert-butyl alcohol; aq. phosphate buffer / 0.13 h / 20 °C / pH 7.2 / Inert atmosphere

With 1H-imidazole; potassium permanganate; sodium periodate; In tetrahydrofuran; aq. phosphate buffer; tert-butyl alcohol;
DOI:10.1016/j.tet.2013.02.008

Reference yield:

: 1449419-19-5
C₁₆H₂₄O₃S₂

: 1449419-31-1
C₄₈H₆₈O₉Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran; toluene / 21 h / 0 - 20 °C

2.1: sodium hydroxide / tetrahydrofuran; water; methanol / 12 h / 0 - 20 °C

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C

3.2: 21.5 h / 0 - 20 °C

4.1: sodium hydrogencarbonate; methyl iodide / acetonitrile; water / 19 h / 20 °C

5.1: sodium dihydrogenphosphate; 2-methyl-but-2-ene; sodium chlorite / tetrahydrofuran; water; tert-butyl alcohol / 0.5 h / 4 °C

6.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / toluene / 3 h / 20 °C

6.2: 1.5 h / 50 °C

7.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 1 h / 20 °C

8.1: 1H-imidazole / tetrahydrofuran / 4 h / 20 °C

9.1: sodium periodate; potassium permanganate / tert-butyl alcohol; aq. phosphate buffer / 0.13 h / 20 °C / pH 7.2 / Inert atmosphere

With 1H-imidazole; sodium chlorite; potassium permanganate; sodium periodate; sodium dihydrogenphosphate; 2-methyl-but-2-ene; di-isopropyl azodicarboxylate; 2,4,6-trichlorobenzoyl chloride; sodium hydride; sodium hydrogencarbonate; triethylamine; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide; methyl iodide; In tetrahydrofuran; methanol; aq. phosphate buffer; dichloromethane; water; toluene; acetonitrile; mineral oil; tert-butyl alcohol; 1.1: |Mitsunobu Displacement / 6.1: |Yamaguchi Lactonization / 6.2: |Yamaguchi Lactonization;
DOI:10.1016/j.tet.2013.02.008