Technology Process of C30H26FN3O4
There total 7 articles about C30H26FN3O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium phosphate; 1,1'-bis(diphenylphosphino)ferrocene-palladium(II)dichloride dichloromethane complex;
In
1,4-dioxane;
at 100 ℃;
for 6h;
DOI:10.1016/j.bmcl.2011.11.113
- Guidance literature:
-
Multi-step reaction with 6 steps
1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 12 h / 80 °C
2: 2,2,6,6-tetramethylpiperidinylmagnesium chloride lithium chloride complex / tetrahydrofuran / 2 h / -30 °C
3: acetic acid; zinc / 1 h
4: triethylsilane; trifluoroacetic acid / dichloromethane / 1 h
5: lithium hexamethyldisilazane / tetrahydrofuran / 3 h / 0 °C
6: potassium phosphate; 1,1'-bis(diphenylphosphino)ferrocene-palladium(II)dichloride dichloromethane complex / 1,4-dioxane / 6 h / 100 °C
With
triethylsilane; potassium phosphate; 2,2,6,6-tetramethylpiperidinylmagnesium chloride lithium chloride complex; 1,1'-bis(diphenylphosphino)ferrocene-palladium(II)dichloride dichloromethane complex; acetic acid; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; lithium hexamethyldisilazane; zinc;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.11.113
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylsilane; trifluoroacetic acid / dichloromethane / 1 h
2: lithium hexamethyldisilazane / tetrahydrofuran / 3 h / 0 °C
3: potassium phosphate; 1,1'-bis(diphenylphosphino)ferrocene-palladium(II)dichloride dichloromethane complex / 1,4-dioxane / 6 h / 100 °C
With
triethylsilane; potassium phosphate; 1,1'-bis(diphenylphosphino)ferrocene-palladium(II)dichloride dichloromethane complex; trifluoroacetic acid; lithium hexamethyldisilazane;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane;
DOI:10.1016/j.bmcl.2011.11.113
