Technology Process of C11H10F2N2*ClH
There total 5 articles about C11H10F2N2*ClH which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C11H8F2N2O;
With
dimethylsulfide borane complex;
In
tetrahydrofuran;
Inert atmosphere;
Reflux;
With
hydrogenchloride;
In
tetrahydrofuran; water;
for 0.5h;
Reflux;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: pyridine hydrochloride / 1,4-dioxane / Reflux
2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; ammonia / water
3.1: dimethylsulfide borane complex / tetrahydrofuran / Inert atmosphere; Reflux
3.2: Reflux
With
dimethylsulfide borane complex; ammonia; pyridine hydrochloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
tetrahydrofuran; 1,4-dioxane; water;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; ammonia / water
2.1: dimethylsulfide borane complex / tetrahydrofuran / Inert atmosphere; Reflux
2.2: Reflux
With
dimethylsulfide borane complex; ammonia; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
tetrahydrofuran; water;